N-[2-(1-benzyl-1H-1,2,3-triazol-4-yl)ethyl]-N-methylamine

Base Information

• Chemical Name: N-[2-(1-benzyl-1H-1,2,3-triazol-4-yl)ethyl]-N-methylamine
• CAS No.: 933719-82-5
• Molecular Formula: C₁₂H₁₆N₄
• Molecular Weight: 216.286
• Mol file: 933719-82-5.mol

Synonyms:

Chemical Property of N-[2-(1-benzyl-1H-1,2,3-triazol-4-yl)ethyl]-N-methylamine

Chemical Property:

• Boiling Point: 386.7±44.0 °C(Predicted)
• PKA: 9.58±0.10(Predicted)
• Density: 1.12±0.1 g/cm3(Predicted)

Purity/Quality:

98%min ^*data from raw suppliers

N-[2-(1-Benzyl-1H-1,2,3-triazol-4-yl)ethyl]-N-methylamine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

Useful:

Technology Process of N-[2-(1-benzyl-1H-1,2,3-triazol-4-yl)ethyl]-N-methylamine

There total 3 articles about N-[2-(1-benzyl-1H-1,2,3-triazol-4-yl)ethyl]-N-methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-(tert-butoxycarbonyl)-N-[2-(1-benzyl-1H-1,2,3-triazol-4-yl)ethyl]-N-methylamine → N-[2-(1-benzyl-1H-1,2,3-triazol-4-yl)ethyl]-N-methylamine (933719-82-5)

Guidance literature:

With phosphoric acid; In dichloromethane; at 20 ℃;

DOI:10.1016/j.bmc.2016.06.045

Reference yield:

benzyl bromide (100-39-0) → N-[2-(1-benzyl-1H-1,2,3-triazol-4-yl)ethyl]-N-methylamine (933719-82-5)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium azide; sodium carbonate; ascorbic acid; copper(ll) sulfate pentahydrate / water; N,N-dimethyl-formamide / 20 °C

2: sodium hydride / mineral oil; tetrahydrofuran / 3 h / 0 - 20 °C

3: phosphoric acid / dichloromethane / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; phosphoric acid; sodium hydride; sodium carbonate; ascorbic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

DOI:10.1016/j.bmc.2016.06.045

Reference yield:

N-(tert-butoxycarbonyl)-N-[2-(1-benzyl-1H-1,2,3-triazol-4-yl)ethyl]amine → N-[2-(1-benzyl-1H-1,2,3-triazol-4-yl)ethyl]-N-methylamine (933719-82-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / mineral oil; tetrahydrofuran / 3 h / 0 - 20 °C

2: phosphoric acid / dichloromethane / 20 °C

With phosphoric acid; sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;

DOI:10.1016/j.bmc.2016.06.045

upstream raw materials:

benzyl bromide

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