1,1,2,2-tetra-t-butyl-1,2-dimethyldigermane

Base Information

• Chemical Name: 1,1,2,2-tetra-t-butyl-1,2-dimethyldigermane
• CAS No.: 82236-90-6
• Molecular Formula: C₁₈H₄₂Ge₂
• Molecular Weight: 403.711

Synonyms:

Chemical Property of 1,1,2,2-tetra-t-butyl-1,2-dimethyldigermane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 1,1,2,2-tetra-t-butyl-1,2-dimethyldigermane

There total 1 articles about 1,1,2,2-tetra-t-butyl-1,2-dimethyldigermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

germaniumtetrachloride (10038-98-9) → 1,1,2,2-tetra-t-butyl-1,2-dimethyldigermane (82236-90-6) + dichloro-di-tert-butylgermane (82236-89-3) + tert-butyltrichlorogermane (1184-92-5)

Guidance literature:

With tert.-butyl lithium; In Petroleum ether; pentane; byproducts: hexa-t-butyldigermane, 1,1,1,2,2-penta-t-butyldigermane; a 15% soln. of t-BuLi in pentane was added dropwise under anhyd. conditions to GeCl4 (2:1 molar ratio) in petroleum ether with a rate to maintain a slight reflux of the mixt., mixt. was stirred at room temp. for 2 d; soln. was filtered, washed, solvents were distilled off, residue distilled in vacuo; elem. anal. for t-Bu2GeCl2, t-BuGeCl3 was identified by its b. p., other minor products - by their mass spectra;

DOI:10.1016/S0022-328X(00)84322-3

upstream raw materials:

germaniumtetrachloride

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