Columbianadin

Base Information

Chemical Name:Columbianadin
CAS No.:3173-03-3
Molecular Formula:C₁₉H₂₀O₅
Molecular Weight:328.365
Hs Code.:

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Suppliers and Price of Columbianadin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 0 raw suppliers

Chemical Property of Columbianadin

Chemical Property:

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Technology Process of Columbianadin

There total 3 articles about Columbianadin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 3804-70-4
columbianetin

: 94487-74-8
(Z)-2-methyl-2-butenoic anhydride

: 3173-03-3,5058-13-9,20414-80-6,21974-14-1,58001-84-6
Columbianadin

Guidance literature:: With caesium carbonate; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1055/s-0032-1317415

Reference yield:

: 565-63-9
Angelic acid

: 3173-03-3,5058-13-9,20414-80-6,21974-14-1,58001-84-6
Columbianadin

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / dichloromethane; 5,5-dimethyl-1,3-cyclohexadiene / 1 h / 20 °C

2: caesium carbonate / acetonitrile / 1 h / 20 °C

With caesium carbonate; dicyclohexyl-carbodiimide; In 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; acetonitrile;
DOI:10.1055/s-0032-1317415