ent-1α,13-diacetoxy-10-hydroxy-3β-thiobenzoyloxy-20-norgibberell-16-ene-7,19-dioic acid 7-methyl ester 19,10-lactone

Base Information

Chemical Name:ent-1α,13-diacetoxy-10-hydroxy-3β-thiobenzoyloxy-20-norgibberell-16-ene-7,19-dioic acid 7-methyl ester 19,10-lactone
CAS No.:81827-02-3
Molecular Formula:C₃₁H₃₄O₉S
Molecular Weight:582.672
Hs Code.:

Synonyms:

Suppliers and Price of ent-1α,13-diacetoxy-10-hydroxy-3β-thiobenzoyloxy-20-norgibberell-16-ene-7,19-dioic acid 7-methyl ester 19,10-lactone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ent-1α,13-diacetoxy-10-hydroxy-3β-thiobenzoyloxy-20-norgibberell-16-ene-7,19-dioic acid 7-methyl ester 19,10-lactone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ent-1α,13-diacetoxy-10-hydroxy-3β-thiobenzoyloxy-20-norgibberell-16-ene-7,19-dioic acid 7-methyl ester 19,10-lactone

There total 1 articles about ent-1α,13-diacetoxy-10-hydroxy-3β-thiobenzoyloxy-20-norgibberell-16-ene-7,19-dioic acid 7-methyl ester 19,10-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2397-26-4
N,N-dimethyl(chlorophenylmethylene)ammonium chloride

: 81827-01-2
C₂₄H₃₀O₉

: 15482-60-7
N,N-dimethylthiobenzamide

: 81827-02-3
ent-1α,13-diacetoxy-10-hydroxy-3β-thiobenzoyloxy-20-norgibberell-16-ene-7,19-dioic acid 7-methyl ester 19,10-lactone

Guidance literature:: With pyridine; ent-1α,13-diacetoxy-3α,10-dihydroxy-20-norgibberell-16-ene-7,19-dioic acid 7-methyl ester 19,10-lactone; hydrogen sulfide; N-ethyl-N,N-diisopropylamine; Yield given. Multistep reaction; 1.) dichloromethane, room temperature, 64 h; 2.) 5 min;

Reference yield:

: 81827-02-3
ent-1α,13-diacetoxy-10-hydroxy-3β-thiobenzoyloxy-20-norgibberell-16-ene-7,19-dioic acid 7-methyl ester 19,10-lactone

: 81826-97-3
gibberellin A₆₀

Guidance literature:: Multi-step reaction with 3 steps

1: 90 mg / bis(tri-n-butylstannyl) oxide, 2,2'-azobis-(2-methylpropiononitrile), polymethylhydrosiloxane / toluene / 4 h / Heating

2: 63 mg / potassium carbonate / methanol / 16 h / Ambient temperature

3: 13 mg / potassium hydroxide, water / methanol / 22 h / Heating

With potassium hydroxide; polymethylhydrosiloxane; 2,2'-azobis(isobutyronitrile); water; potassium carbonate; bis(tri-n-butyltin)oxide; In methanol; toluene;