(diacetyl hydrogenato-kappaO borate)[2-({[2-(sulfanyl-kappaS)phenyl]imino-kappaN}methyl)phenolato(2-)-kappaO]boron

Base Information

• Chemical Name: (diacetyl hydrogenato-kappaO borate)[2-({[2-(sulfanyl-kappaS)phenyl]imino-kappaN}methyl)phenolato(2-)-kappaO]boron
• CAS No.: 85561-03-1
• Molecular Formula: C₁₇H₁₅B₂NO₆S
• Molecular Weight: 382.997
• Mol file: 85561-03-1.mol

Synonyms:

Chemical Property of (diacetyl hydrogenato-kappaO borate)[2-({[2-(sulfanyl-kappaS)phenyl]imino-kappaN}methyl)phenolato(2-)-kappaO]boron

Chemical Property:

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (diacetyl hydrogenato-kappaO borate)[2-({[2-(sulfanyl-kappaS)phenyl]imino-kappaN}methyl)phenolato(2-)-kappaO]boron

There total 1 articles about (diacetyl hydrogenato-kappaO borate)[2-({[2-(sulfanyl-kappaS)phenyl]imino-kappaN}methyl)phenolato(2-)-kappaO]boron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetraacetyl diborate (5187-37-1) + 2-(2-hydroxyphenyl)benzothiazoline (7361-94-6) → C13H9NOSBOB(OCOCH3)2 (85561-03-1)

Guidance literature:

In toluene; to a soln. of O(B(OAc)2)2 benzothiazoline (molar ratio 1:1) was aded; amixture was refluxed for 12 h, acetic acid liberated being removed azeotripically; concn., residue was dried at 60-65°C/0.05 torr; repeatedly washed with dry hexane; elem. anal.;

upstream raw materials:

tetraacetyl diborate

2-(2-hydroxyphenyl)benzothiazoline