Methanethiol, bis(trimethylsilyl)-

Base Information

Chemical Name:Methanethiol, bis(trimethylsilyl)-
CAS No.:99405-17-1
Molecular Formula:C7H20 S Si2
Molecular Weight:192.473
Hs Code.:
DSSTox Substance ID:DTXSID70244055
Wikidata:Q83128329

Synonyms:Methanethiol, bis(trimethylsilyl)-;99405-17-1;Bis(trimethylsilyl)methanethiol;DTXSID70244055

Suppliers and Price of Methanethiol, bis(trimethylsilyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanethiol, bis(trimethylsilyl)-

Chemical Property:

Vapor Pressure:1.61mmHg at 25°C
Boiling Point:174.5°C at 760 mmHg
Flash Point:59.3°C
Density:0.836g/cm³
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:192.08242488
Heavy Atom Count:10
Complexity:95.8

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)C([Si](C)(C)C)S

Technology Process of Methanethiol, bis(trimethylsilyl)-

There total 3 articles about Methanethiol, bis(trimethylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 98351-26-9
bis(trimethylsilyl)methyl trimethylsilyl sulfide

: 99405-17-1
bis(trimethylsilyl)methanethiol

Guidance literature:: With sulfuric acid; In tetrahydrofuran; at 25 ℃; for 0.5h;
DOI:10.1016/S0040-4039(00)95068-8

Reference yield:

: 1068-69-5
Tris(trimethylsilyl)methane

: 99405-17-1
bis(trimethylsilyl)methanethiol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) methyllithium; 2.) elemental sulfur / 1.) THF, reflux, 16 h; 2.) 25 deg C, 2 h

2: 100 percent / 7 h / 230 - 240 °C

3: 85 percent / 1 M sulfuric acid / tetrahydrofuran / 0.5 h / 25 °C

With sulfuric acid; methyllithium; sulfur; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)95068-8

Reference yield:

: 98195-03-0
Tris(trimethylsilyl)methylsulfane

: 99405-17-1
bis(trimethylsilyl)methanethiol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 7 h / 230 - 240 °C

2: 85 percent / 1 M sulfuric acid / tetrahydrofuran / 0.5 h / 25 °C

With sulfuric acid; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)95068-8