VCl₃(tetrahydrofuran)₃

Base Information

Chemical Name:VCl₃(tetrahydrofuran)₃
CAS No.:1372665-07-0
Molecular Formula:C₁₂H₂₄Cl₃O₃V
Molecular Weight:373.621
Hs Code.:

VCl<sub>3</sub>(tetrahydrofuran)<sub>3</sub>

Synonyms:

Suppliers and Price of VCl₃(tetrahydrofuran)₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of VCl₃(tetrahydrofuran)₃

Chemical Property:

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Technology Process of VCl₃(tetrahydrofuran)₃

There total 3 articles about VCl₃(tetrahydrofuran)₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 7632-51-1
vanadiumtetrachloride

: 131063-11-1,1372665-07-0,16997-51-6,19559-06-9
VCl₃(tetrahydrofuran)₃

Guidance literature:: With triethylboron; In dichloromethane; under Ar or N2; THF was cooled in an ice bath, VCl4 in CH2Cl2 was added, BEt3 was added, warmed to 90°C (oil bath) for 1 h; cooling, filtn., washing, drying in a glovebox;

Reference yield: 58.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 12081-36-6
vanadium (IV) chloride * 2 tetrahydrofurane

: 7440-66-6
zinc

: 131063-11-1,1372665-07-0,16997-51-6,19559-06-9
VCl₃(tetrahydrofuran)₃

: 93530-27-9
VCl₂(C₄OH₈)4⁽¹⁺⁾*ZnCl₃(C₄OH₈)^(1-)=(VCl₂(C₄OH₈)4)(ZnCl₃(C₄OH₈))

Guidance literature:: In tetrahydrofuran; under Ar or N2; a mixt. of the V complex and Zn dust was cooled in an ice bath, THF was added, warming in an oil bath to 80°C for 1 h; filtn., refluxing the crystals in THF, filtered hot, extg. of the green solid with THF, filtn.;