N-(3-chloro-5-methoxyphenyl)acetohydroxamsaeure

Base Information

• Chemical Name: N-(3-chloro-5-methoxyphenyl)acetohydroxamsaeure
• CAS No.: 117970-20-4
• Molecular Formula: C₉H₁₀ClNO₃
• Molecular Weight: 215.636
• Mol file: 117970-20-4.mol

Synonyms:

Chemical Property of N-(3-chloro-5-methoxyphenyl)acetohydroxamsaeure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N-(3-chloro-5-methoxyphenyl)acetohydroxamsaeure

There total 1 articles about N-(3-chloro-5-methoxyphenyl)acetohydroxamsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloro-3,5-dinitrobenzene (618-86-0) → N-(3-chloro-5-methoxyphenyl)acetohydroxamsaeure (117970-20-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 57 percent / Na / 70 h / 80 °C

2: 1.) H₂/Pt/C; 2.) NaHCO₃ / 1.) THF, DMSO, NH₃, H₂O; 15 deg C; 1.5 h; 2.) H₂O, THF; 0 deg C; 30 min

With platinum on activated charcoal; hydrogen; sodium; sodium hydrogencarbonate;

DOI:10.1002/hlca.19880710206

Reference yield:

vinyl acetate (108-05-4,9003-20-7) + N-(3-chloro-5-methoxyphenyl)acetohydroxamsaeure (117970-20-4) → 4-chlor-6-methoxyindol (93490-31-4) + 6-chlor-4-methoxyindol

Guidance literature:

With potassium hydroxide; lithium tetrachloropalladate(II); Yield given. Multistep reaction. Yields of byproduct given; 1.)50 deg C, 3 h; 2.) 20 deg C, 30 min, methanol;

DOI:10.1002/hlca.19880710206

upstream raw materials:

1-chloro-3,5-dinitrobenzene

Downstream raw materials:

4-chlor-6-methoxyindol