2-deoxy-2-fluoro-α-D-glucopyranosyl

Base Information

Chemical Name:2-deoxy-2-fluoro-α-D-glucopyranosyl
CAS No.:109959-19-5
Molecular Formula:C₆H₁₂FO₈P*2C₆H₁₃N
Molecular Weight:460.48
Hs Code.:

2-deoxy-2-fluoro-α-D-glucopyranosyl <bis(cyclohexylammonium) phosphate>

Synonyms:

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Chemical Property of 2-deoxy-2-fluoro-α-D-glucopyranosyl

Chemical Property:

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Technology Process of 2-deoxy-2-fluoro-α-D-glucopyranosyl

There total 5 articles about 2-deoxy-2-fluoro-α-D-glucopyranosyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24679-89-8
trifluoromethyl 3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-α-D-glucopyranoside

: 109959-19-5,109959-21-9
2-deoxy-2-fluoro-β-D-glucopyranosyl

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 45percent HBr, Ac₂O, HOAc / 144 h / Ambient temperature

2: 1) silver triflate, 2) phosphoric acid, 3) Dowex 50W-X₈(1+)> / 1) CH₃CN, 30 min, RT, in dark, 2) 90 min, reflux

With phosphoric acid; Dowex 50W-X8; hydrogen bromide; silver trifluoromethanesulfonate; acetic anhydride; acetic acid;
DOI:10.1016/S0008-6215(00)90028-4

Reference yield:

: 24679-89-8
trifluoromethyl 3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-α-D-glucopyranoside

: 109959-19-5,109959-21-9
2-deoxy-2-fluoro-α-D-glucopyranosyl

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / 45percent HBr, Ac₂O, HOAc / 144 h / Ambient temperature

2: 73 percent / Hg(OAc)2 / 20 h / Ambient temperature

3: 1) phosphoric acid, 2) Dowex 50W-X₈(1+)> / 1) 55 deg C, 48 h

With phosphoric acid; Dowex 50W-X8; mercury(II) diacetate; hydrogen bromide; acetic anhydride; acetic acid;
DOI:10.1016/S0008-6215(00)90028-4

Reference yield:

: 34245-85-7
3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-α-D-glucopyranosyl bromide

: 109959-19-5,109959-21-9
2-deoxy-2-fluoro-α-D-glucopyranosyl

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Hg(OAc)2 / 20 h / Ambient temperature

2: 1) phosphoric acid, 2) Dowex 50W-X₈(1+)> / 1) 55 deg C, 48 h

With phosphoric acid; Dowex 50W-X8; mercury(II) diacetate;
DOI:10.1016/S0008-6215(00)90028-4