C₃₃H₃₄ClNO₁₀

Base Information

Chemical Name:C₃₃H₃₄ClNO₁₀
CAS No.:1311379-36-8
Molecular Formula:C₃₃H₃₄ClNO₁₀
Molecular Weight:640.087
Hs Code.:

C<sub>33</sub>H<sub>34</sub>ClNO<sub>10</sub>

Synonyms:

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Chemical Property of C₃₃H₃₄ClNO₁₀

Chemical Property:

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Technology Process of C₃₃H₃₄ClNO₁₀

There total 14 articles about C₃₃H₃₄ClNO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₃₆ClNO₁₁

: 1311379-36-8
C₃₃H₃₄ClNO₁₀

Guidance literature:: With pyridine; 1,3,5-trichloro-2,4,6-triazine; In 1,2-dichloro-ethane; at 20 - 75 ℃; for 1.08333h; Inert atmosphere;
DOI:10.1021/ja203642n

Reference yield:

: C₁₇H₂₀O₄

: 1311379-36-8
C₃₃H₃₄ClNO₁₀

Guidance literature:: Multi-step reaction with 11 steps

1: sodium chlorite; sodium phosphate monobasic monohydrate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 °C

2: sulfuric acid / 0 - 20 °C / Inert atmosphere

3: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere

4: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating

5: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere

6: magnesium iodide / dichloromethane / -78 - -20 °C / Inert atmosphere

7: boron trichloride / dichloromethane / 1 h / -78 °C / Inert atmosphere

8: 10-camphorsufonic acid / dichloromethane / 1 h / 40 °C / Inert atmosphere; Sonication

9: potassium phosphate / dimethyl sulfoxide / 50 °C / Inert atmosphere

10: lithium hydroxide monohydrate; water / 1,4-dioxane / 75 °C / Inert atmosphere

11: pyridine; 1,3,5-trichloro-2,4,6-triazine / 1,2-dichloro-ethane / 1.08 h / 20 - 75 °C / Inert atmosphere

With pyridine; sodium chlorite; potassium phosphate; chloro-trimethyl-silane; 1,3,5-trichloro-2,4,6-triazine; sodium phosphate monobasic monohydrate; lithium hydroxide monohydrate; sulfuric acid; 10-camphorsufonic acid; water; boron trichloride; sodium cyanoborohydride; toluene-4-sulfonic acid; magnesium iodide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 1,4-dioxane; 2-methyl-but-2-ene; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; 1,2-dichloro-ethane; acetonitrile; tert-butyl alcohol; 1: Pinnick oxidation / 6: intramolecular halo-Michael aldol reaction;
DOI:10.1021/ja203642n

Reference yield:

: C₁₇H₂₀O₅

: 1311379-36-8
C₃₃H₃₄ClNO₁₀

Guidance literature:: Multi-step reaction with 10 steps

1: sulfuric acid / 0 - 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere

3: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating

4: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere

5: magnesium iodide / dichloromethane / -78 - -20 °C / Inert atmosphere

6: boron trichloride / dichloromethane / 1 h / -78 °C / Inert atmosphere

7: 10-camphorsufonic acid / dichloromethane / 1 h / 40 °C / Inert atmosphere; Sonication

8: potassium phosphate / dimethyl sulfoxide / 50 °C / Inert atmosphere

9: lithium hydroxide monohydrate; water / 1,4-dioxane / 75 °C / Inert atmosphere

10: pyridine; 1,3,5-trichloro-2,4,6-triazine / 1,2-dichloro-ethane / 1.08 h / 20 - 75 °C / Inert atmosphere

With pyridine; potassium phosphate; chloro-trimethyl-silane; 1,3,5-trichloro-2,4,6-triazine; lithium hydroxide monohydrate; sulfuric acid; 10-camphorsufonic acid; water; boron trichloride; sodium cyanoborohydride; toluene-4-sulfonic acid; magnesium iodide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 1,4-dioxane; dichloromethane; dimethyl sulfoxide; ethyl acetate; 1,2-dichloro-ethane; acetonitrile; 5: intramolecular halo-Michael aldol reaction;
DOI:10.1021/ja203642n