Butanoic acid, (3-oxo-2-phenyl-5-isoxazolidinyl)methyl ester, (R)-

Base Information

Chemical Name:Butanoic acid, (3-oxo-2-phenyl-5-isoxazolidinyl)methyl ester, (R)-
CAS No.:140384-94-7
Molecular Formula:C14H17NO4
Molecular Weight:263.293
Hs Code.:

Synonyms:

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Chemical Property of Butanoic acid, (3-oxo-2-phenyl-5-isoxazolidinyl)methyl ester, (R)-

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Technology Process of Butanoic acid, (3-oxo-2-phenyl-5-isoxazolidinyl)methyl ester, (R)-

There total 6 articles about Butanoic acid, (3-oxo-2-phenyl-5-isoxazolidinyl)methyl ester, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-65-2
N-Phenylhydroxylamine

: 140384-94-7
Butyric acid (R)-3-oxo-2-phenyl-isoxazolidin-5-ylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: diethyl ether / 0.25 h

2: 48 percent / aq. sodium bicarbonate / diethyl ether / Ambient temperature

3: 61 percent / NaBH₄, LiCl / tetrahydrofuran; methanol / 0.17 h

4: pyridine / CH₂Cl₂

5: potassium phosphate buffer, pH 7 / lipase PS / acetone / Ambient temperature

With pyridine; sodium tetrahydroborate; potassium phosphate buffer; sodium hydrogencarbonate; lithium chloride; Lipase PS; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetone;
DOI:10.1021/jo00036a013

Reference yield:

: 140176-83-6
benzyl (+/-)-2-phenyl-3-oxo-5-isoxazolidinecarboxylate

: 140384-94-7
Butyric acid (R)-3-oxo-2-phenyl-isoxazolidin-5-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / NaBH₄, LiCl / tetrahydrofuran; methanol / 0.17 h

2: pyridine / CH₂Cl₂

3: potassium phosphate buffer, pH 7 / lipase PS / acetone / Ambient temperature

With pyridine; sodium tetrahydroborate; potassium phosphate buffer; lithium chloride; Lipase PS; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1021/jo00036a013

Reference yield:

: 3-(benzyloxycarbonyl)-3-chloro-N-phenylpropiono-N-hydroxamic acid

: 140384-94-7
Butyric acid (R)-3-oxo-2-phenyl-isoxazolidin-5-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 48 percent / aq. sodium bicarbonate / diethyl ether / Ambient temperature

2: 61 percent / NaBH₄, LiCl / tetrahydrofuran; methanol / 0.17 h

3: pyridine / CH₂Cl₂

4: potassium phosphate buffer, pH 7 / lipase PS / acetone / Ambient temperature

With pyridine; sodium tetrahydroborate; potassium phosphate buffer; sodium hydrogencarbonate; lithium chloride; Lipase PS; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetone;
DOI:10.1021/jo00036a013