2-aminoethyl nitrate nitrate (1:1)

Base Information

• Chemical Name: 2-aminoethyl nitrate nitrate (1:1)
• CAS No.: 133300-54-6
• Molecular Formula: C₂H₆N₂O₃*HNO₃
• Molecular Weight: 169.094
• Mol file: 133300-54-6.mol

Synonyms:

Chemical Property of 2-aminoethyl nitrate nitrate (1:1)

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-aminoethyl nitrate nitrate (1:1)

There total 2 articles about 2-aminoethyl nitrate nitrate (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ethanolamine (141-43-5) → 2-nitroxyethylammonium nitrate (4665-58-1,133300-54-6)

Guidance literature:

ethanolamine; With nitric acid; In dichloromethane; at 0 ℃; for 0.833333h;

With acetic anhydride; In dichloromethane; at 20 ℃; for 0.666667h;

Reference yield:

→ 2-nitroxyethylammonium nitrate (4665-58-1,133300-54-6)

Guidance literature:

Reference yield:

2-nitroxyethylammonium nitrate (4665-58-1,133300-54-6) + (2R,4R)-3-(Ethoxycarbonyl)-2-phenyl-1,3-thiazolidine-4-carboxylic acid (161153-14-6) → (2R,4R)-2-phenyl-3-(carbethoxy)thiazolidine-4-carboxamide

Guidance literature:

With chloroformic acid ethyl ester; triethylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) CH₂Cl₂, 15 deg C, 1 h;

DOI:10.1002/jhet.5570310608

upstream raw materials:

ethanolamine