1-(2-CHLOROPHENYL)METHYLENEIMMONIUM-3-PYRAZOLIDINONE-1,2-INNER SALT

Base Information

Chemical Name:1-(2-CHLOROPHENYL)METHYLENEIMMONIUM-3-PYRAZOLIDINONE-1,2-INNER SALT
CAS No.:1164110-98-8
Molecular Formula:C₁₀H₉ClN₂O
Molecular Weight:208.647
Hs Code.:
Mol file:1164110-98-8.mol

Synonyms:

Suppliers and Price of 1-(2-CHLOROPHENYL)METHYLENEIMMONIUM-3-PYRAZOLIDINONE-1,2-INNER SALT

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

American Custom Chemicals Corporation
1-(2-CHLOROPHENYL)METHYLENEIMMONIUM-3-PYRAZOLIDINONE-1,2-INNER SALT 95.00%
10MG
$ 679.14

Total 0 raw suppliers

Chemical Property of 1-(2-CHLOROPHENYL)METHYLENEIMMONIUM-3-PYRAZOLIDINONE-1,2-INNER SALT

Chemical Property:

Purity/Quality:: 1-(2-CHLOROPHENYL)METHYLENEIMMONIUM-3-PYRAZOLIDINONE-1,2-INNER SALT 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(2-CHLOROPHENYL)METHYLENEIMMONIUM-3-PYRAZOLIDINONE-1,2-INNER SALT

There total 3 articles about 1-(2-CHLOROPHENYL)METHYLENEIMMONIUM-3-PYRAZOLIDINONE-1,2-INNER SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 10234-72-7
pyrazolidin-3-one

: 89-98-5
2-chloro-benzaldehyde

: 1164110-98-8
2-(2-chlorobenzylidene)-5-oxopyrazolidin-2-ium-1-ide

Guidance literature:: With hydrazine hydrate; In methanol; at 20 ℃; for 8h; Reflux;
DOI:10.1021/acs.orglett.6b01104

Reference yield:

: 89-98-5
2-chloro-benzaldehyde

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1164110-98-8
2-(2-chlorobenzylidene)-5-oxopyrazolidin-2-ium-1-ide

Guidance literature:: acrylic acid methyl ester; With hydrazine hydrate; In ethanol; at 78 ℃; Inert atmosphere;

2-chloro-benzaldehyde; In methanol; at 20 ℃; Inert atmosphere;
DOI:10.1039/c3cc41119b

Reference yield:

: 1752-88-1
tetrahydro-3H-pyrazol-3-one hydrochloride

: 89-98-5
2-chloro-benzaldehyde

: 1164110-98-8
2-(2-chlorobenzylidene)-5-oxopyrazolidin-2-ium-1-ide

Guidance literature:: tetrahydro-3H-pyrazol-3-one hydrochloride; With magnesium sulfate; triethylamine; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;

2-chloro-benzaldehyde; In dichloromethane; at 0 - 20 ℃; for 48h; Inert atmosphere;
DOI:10.1002/anie.201307317