Technology Process of 3,4,4a,10,11,11a-esaidro-2H,5H-benzo<5,6>cicloept<1,2-b><1,4>ossazina
There total 6 articles about 3,4,4a,10,11,11a-esaidro-2H,5H-benzo<5,6>cicloept<1,2-b><1,4>ossazina which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
benzene;
1.) 5 deg C, 1 h, 2.) 1 h, room temp., 3.) 1.5 h, reflux;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 84.5 percent / AmONO / methanol; HCl / 1.) -5 deg C, 30 min, 2.) 0 deg C, 1 h
2: 20percent aq. HCl
3: 60 percent / hydrogen / 10percent Pd/BaSO4 / acetic acid / Ambient temperature
4: 94 percent / NaBH4 / methanol; H2O / Ambient temperature
5: 82 percent / 2N NaOH / methanol / Heating
6: 89 percent / NaH / benzene / 1.) 5 deg C, 1 h, 2.) 1 h, room temp., 3.) 1.5 h, reflux
With
hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; hydrogen; sodium hydride;
Pd-BaSO4;
In
hydrogenchloride; methanol; water; acetic acid; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 60 percent / hydrogen / 10percent Pd/BaSO4 / acetic acid / Ambient temperature
2: 94 percent / NaBH4 / methanol; H2O / Ambient temperature
3: 82 percent / 2N NaOH / methanol / Heating
4: 89 percent / NaH / benzene / 1.) 5 deg C, 1 h, 2.) 1 h, room temp., 3.) 1.5 h, reflux
With
sodium hydroxide; sodium tetrahydroborate; hydrogen; sodium hydride;
Pd-BaSO4;
In
methanol; water; acetic acid; benzene;
