C₁₄H₁₇IO₄

Base Information

Chemical Name:C₁₄H₁₇IO₄
CAS No.:1597430-75-5
Molecular Formula:C₁₄H₁₇IO₄
Molecular Weight:376.191
Hs Code.:

C<sub>14</sub>H<sub>17</sub>IO<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₇IO₄

Chemical Property:

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Technology Process of C₁₄H₁₇IO₄

There total 1 articles about C₁₄H₁₇IO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 49617-83-6
m-Iodobenzyl bromide

: 105-53-3
diethyl malonate

: 1597430-75-5
C₁₄H₁₇IO₄

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1021/jm500367e

Reference yield:

: 1597430-75-5
C₁₄H₁₇IO₄

: C₁₈H₂₅IN₃O₁₅P₃*C₆H₁₅N

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium chloride / dimethyl sulfoxide

2.1: diisobutylaluminium hydride

3.1: carbon tetrabromide; triphenylphosphine

4.1: triethylamine / N,N-dimethyl-formamide / 100 °C

5.1: hydrazine hydrate

6.1: pyridine / 100 °C

7.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trimethyl phosphite; trichlorophosphate / 2 h / 0 °C

7.2: 0.17 h / 0 °C

7.3: 1 h / 20 °C

With pyridine; trimethyl phosphite; carbon tetrabromide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; diisobutylaluminium hydride; hydrazine hydrate; triethylamine; triphenylphosphine; sodium chloride; trichlorophosphate; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm500367e

Reference yield:

: 1597430-75-5
C₁₄H₁₇IO₄

: 141763-48-6
3-(3-iodophenyl)-1-propanol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium chloride / dimethyl sulfoxide

2: diisobutylaluminium hydride

With diisobutylaluminium hydride; sodium chloride; In dimethyl sulfoxide;
DOI:10.1021/jm500367e