cis-4,7,10,13,16,19-docosahexaenoic acid

Base Information

Chemical Name:cis-4,7,10,13,16,19-docosahexaenoic acid
CAS No.:1095558-71-6
Molecular Formula:C₂₃H₃₄O₂
Molecular Weight:342.522
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-4,7,10,13,16,19-docosahexaenoic acid

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Technology Process of cis-4,7,10,13,16,19-docosahexaenoic acid

There total 6 articles about cis-4,7,10,13,16,19-docosahexaenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1312442-38-8
methyl (5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenoate

: 1095558-71-6
cis-4,7,10,13,16,19-docosahexaenoic acid

Guidance literature:: With potassium hydroxide; In methanol; water; at 50 ℃; for 1h;
DOI:10.1007/s11745-011-3541-5

Reference yield:

: 1312442-36-6
(5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenenitrile

: 1095558-71-6
cis-4,7,10,13,16,19-docosahexaenoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -20 °C / Inert atmosphere

2: iodine; potassium hydroxide / 1 h / 0 °C / Inert atmosphere

3: potassium hydroxide / methanol; water / 1 h / 50 °C

With iodine; diisobutylaluminium hydride; potassium hydroxide; In methanol; dichloromethane; water; toluene;
DOI:10.1007/s11745-011-3541-5

Reference yield:

: 1312442-37-7
(5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenal

: 1095558-71-6
cis-4,7,10,13,16,19-docosahexaenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; potassium hydroxide / 1 h / 0 °C / Inert atmosphere

2: potassium hydroxide / methanol; water / 1 h / 50 °C

With iodine; potassium hydroxide; In methanol; water;
DOI:10.1007/s11745-011-3541-5