methyl (5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenoate

Base Information

Chemical Name:methyl (5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenoate
CAS No.:1312442-38-8
Molecular Formula:C₂₄H₃₆O₂
Molecular Weight:356.549
Hs Code.:

Synonyms:

Suppliers and Price of methyl (5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenoate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of methyl (5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenoate

There total 5 articles about methyl (5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 67-56-1
methanol

: 1312442-37-7
(5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenal

: 1312442-38-8
methyl (5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenoate

Guidance literature:: With iodine; potassium hydroxide; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1007/s11745-011-3541-5

Reference yield:

: 1312442-36-6
(5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenenitrile

: 1312442-38-8
methyl (5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenoate

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -20 °C / Inert atmosphere

2: iodine; potassium hydroxide / 1 h / 0 °C / Inert atmosphere

With iodine; diisobutylaluminium hydride; potassium hydroxide; In dichloromethane; toluene;
DOI:10.1007/s11745-011-3541-5

Reference yield:

: 6217-54-5
docosahexaenoic acid

: 1312442-38-8
methyl (5Z,8Z,11Z,14Z,17Z,20Z)-tricosa-5,8,11,14,17,20-hexaenoate

Guidance literature:: Multi-step reaction with 5 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / 0 °C / Inert atmosphere

2: pyridine / 13 h / 0 °C / Inert atmosphere

3: potassium cyanide / dimethyl sulfoxide / 2.5 h / 70 °C / Inert atmosphere

4: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -20 °C / Inert atmosphere

5: iodine; potassium hydroxide / 1 h / 0 °C / Inert atmosphere

With pyridine; potassium cyanide; iodine; diisobutylaluminium hydride; potassium hydroxide; In dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1007/s11745-011-3541-5