9-(trifluoromethyl)anthracene

Base Information

• Chemical Name: 9-(trifluoromethyl)anthracene
• CAS No.: 120568-02-7
• Molecular Formula: C₁₅H₉F₃
• Molecular Weight: 246.232
• Mol file: 120568-02-7.mol

Synonyms:

Chemical Property of 9-(trifluoromethyl)anthracene

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

9-(Trifluoromethyl)anthracene 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-(trifluoromethyl)anthracene

There total 2 articles about 9-(trifluoromethyl)anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

9-chloroanthracene (716-53-0) + (trifluoromethyl)triethylsilane (120120-26-5) → 9-(trifluoromethyl)anthracene (120568-02-7)

Guidance literature:

With potassium fluoride; [(allyl)PdCl]2; ruphos; In 1,4-dioxane; at 140 ℃;

DOI:10.1126/science.1190524

Reference yield: 80.0%

9-Bromoanthracene (1564-64-3) + (trifluoromethyl)trimethylsilane (81290-20-2) → 9-(trifluoromethyl)anthracene (120568-02-7)

Guidance literature:

With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; sodium dodecyl-sulfate; cesium fluoride; In toluene; at 110 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c1cc12098k

upstream raw materials:

9-chloroanthracene

(trifluoromethyl)triethylsilane

9-Bromoanthracene

(trifluoromethyl)trimethylsilane