Technology Process of uridine 5'-diphospho-2-azido-2-deoxy-α-D-glucopyranoside
There total 6 articles about uridine 5'-diphospho-2-azido-2-deoxy-α-D-glucopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium bicarbonate; triethylamine;
In
methanol; water;
for 14h;
- Guidance literature:
-
With
recombinant Bifidobacterium infantis ATCC15697 N-acetylhexosamine 1-kinase; recombinant Bifidobacterium longum ATCC55813 UDP-sugar pyrophosphorylase; recombinant Pasteurella multocida P-1059 inorganic pyrophosphatase; ATP; magnesium chloride;
at 37 ℃;
for 24h;
pH=8;
aq. buffer;
Enzymatic reaction;
DOI:10.1039/c2cc17577k
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dimethyl amine
2: 2-Chloro-4H-1,3,2-benzodioxaphosphorin-4-one / tetrahydrofuran; 1,4-dioxane
3: tert.-butylhydroperoxide; iodine / tetrahydrofuran / 48 h
4: 1H-tetrazole; pyridine / 24 h
5: triethylamine; ammonium bicarbonate / water; methanol / 14 h
With
pyridine; 1H-tetrazole; tert.-butylhydroperoxide; 2-Chloro-4H-1,3,2-benzodioxaphosphorin-4-one; iodine; ammonium bicarbonate; dimethyl amine; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; methanol; water;
