Technology Process of C27H46O2
There total 3 articles about C27H46O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
methyllithium;
With
cerium(III) chloride;
In
tetrahydrofuran; diethyl ether;
at -78 ℃;
for 1.5h;
Inert atmosphere;
C26H42O2;
In
tetrahydrofuran; diethyl ether;
at -78 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrahydrofuran / 2.25 h / 0 - 20 °C / Inert atmosphere
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane; chloroform / 2.92 h / Inert atmosphere
2.2: 0.42 h / -78 °C
3.1: cerium(III) chloride / tetrahydrofuran; diethyl ether / 1.5 h / -78 °C / Inert atmosphere
3.2: 1 h / -78 °C
With
cerium(III) chloride; oxalyl dichloride; dimethyl sulfoxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; chloroform;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane; chloroform / 2.92 h / Inert atmosphere
1.2: 0.42 h / -78 °C
2.1: cerium(III) chloride / tetrahydrofuran; diethyl ether / 1.5 h / -78 °C / Inert atmosphere
2.2: 1 h / -78 °C
With
cerium(III) chloride; oxalyl dichloride; dimethyl sulfoxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; chloroform;
