3-Ethyl-3H-[1,2,4]triazolo[1,5-a]benzimidazole

Base Information

Chemical Name:3-Ethyl-3H-[1,2,4]triazolo[1,5-a]benzimidazole
CAS No.:124617-74-9
Molecular Formula:C₁₀H₁₀N₄
Molecular Weight:186.216
Hs Code.:
DSSTox Substance ID:DTXSID101245688
Nikkaji Number:J3.641.352B

Synonyms:3-Ethyl-3H-[1,2,4]triazolo[1,5-a]benzimidazole;DTXSID101245688;124617-74-9

Suppliers and Price of 3-Ethyl-3H-[1,2,4]triazolo[1,5-a]benzimidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Ethyl-3H-[1,2,4]triazolo[1,5-a]benzimidazole

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:186.090546336
Heavy Atom Count:14
Complexity:220

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCN1C=NN2C1=NC3=CC=CC=C32

Technology Process of 3-Ethyl-3H-[1,2,4]triazolo[1,5-a]benzimidazole

There total 12 articles about 3-Ethyl-3H-[1,2,4]triazolo[1,5-a]benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 64-67-5
diethyl sulfate

: 41029-35-0
1,2,4-Triazolo<1,5-a>benzimidazole

: 124617-74-9
3-Ethyl-3H-1,2,4-triazolo<1,5-a>benzimidazole

Guidance literature:: at 140 - 150 ℃; for 0.5h; Product distribution;
DOI:10.1007/BF00479912

Reference yield: 84.0%

: 1-(2-azidophenyl)-4-ethyl-1,2,4-triazolium iodide

: 124617-74-9
3-Ethyl-3H-1,2,4-triazolo<1,5-a>benzimidazole

Guidance literature:: With ammonium hydroxide; copper(l) chloride; In ethanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c6cc09160a

Reference yield:

: 934-32-7
1H-benzimidazol-2-amine

: 124617-74-9
3-Ethyl-3H-1,2,4-triazolo<1,5-a>benzimidazole

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / hydroxylamine-O-sulfonic acid, KOH / H₂O / 0.5 h / 40 - 45 °C

2: 66 percent / 0.5 h / Heating

3: 94 percent / 2 h / Heating

4: 82 percent / CH₂Cl₂ / 24 h / 20 °C

5: 22percent NH₄OH

With potassium hydroxide; ammonium hydroxide; hydroxylamine-O-sulfonic acid; In dichloromethane; water;
DOI:10.1007/BF00479912