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threo-1-phenyl-2-(phenylseleno)-3-buten-1-ol

Base Information
  • Chemical Name:threo-1-phenyl-2-(phenylseleno)-3-buten-1-ol
  • CAS No.:88916-10-3
  • Molecular Formula:C16H16OSe
  • Molecular Weight:303.262
  • Hs Code.:
threo-1-phenyl-2-(phenylseleno)-3-buten-1-ol

Synonyms:

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of threo-1-phenyl-2-(phenylseleno)-3-buten-1-ol
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Technology Process of threo-1-phenyl-2-(phenylseleno)-3-buten-1-ol

There total 2 articles about threo-1-phenyl-2-(phenylseleno)-3-buten-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: 1.) NaBH4 / 1.) ethanol, room temperature, 30 min
2: 1.) lithium diisopropylamide, 2.) triethylaluminum
With sodium tetrahydroborate; triethylaluminum; lithium diisopropyl amide;
DOI:10.1021/jo00180a027
Guidance literature:
With lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 30 min, 2.) -78 deg C up to room temperature;
DOI:10.1021/jo00180a027
Guidance literature:
With toluene-4-sulfonic acid;
DOI:10.1021/jo00180a027
upstream raw materials:

allyl phenyl selenide

benzaldehyde

diphenyl diselenide

Downstream raw materials:

(E)-buta-1,3-dienylbenzene

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