C₅₀H₈₆N₁₂O₁₀

Base Information

• Chemical Name: C₅₀H₈₆N₁₂O₁₀
• CAS No.: 916728-33-1
• Molecular Formula: C₅₀H₈₆N₁₂O₁₀
• Molecular Weight: 1015.31
• Mol file: 916728-33-1.mol

Synonyms:

Chemical Property of C₅₀H₈₆N₁₂O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₀H₈₆N₁₂O₁₀

There total 5 articles about C₅₀H₈₆N₁₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3'-Diamino-N-methyldipropylamine (105-83-9) → C50H86N12O10 (916728-33-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 74 percent / dioxane / 4 h / Heating

2: 72 percent / diethyl ether / 12 h / 20 °C

3: 214 mg / ethanol / 15 h / 20 °C

In 1,4-dioxane; diethyl ether; ethanol;

DOI:10.1002/anie.200602790

Reference yield:

N-(3-aminopropyl)-N-(3-tert-butyloxycarbonyl-aminopropyl)-N-methylamine (87530-14-1) → C50H86N12O10 (916728-33-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / diethyl ether / 12 h / 20 °C

2: 214 mg / ethanol / 15 h / 20 °C

In diethyl ether; ethanol;

DOI:10.1002/anie.200602790

Reference yield:

(3-{[3-(2-{3-[(3-tert-butoxycarbonylamino-propyl)-methyl-amino]-propylamino}-3,4-dioxo-cyclobut-1-enylamino)-propyl]-methyl-amino}-propyl)-carbamic acid tert-butyl ester (916728-31-9) → C50H86N12O10 (916728-33-1)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl / H₂O / 4 h / 50 °C

2: 214 mg / ethanol / 15 h / 20 °C

With hydrogenchloride; In ethanol; water;

DOI:10.1002/anie.200602790

upstream raw materials:

(3-{[3-(2-ethoxy-3,4-dioxo-cyclobut-1-enylamino)-propyl]-methyl-amino}-propyl)-carbamic acid tert-butyl ester

(3-{[3-(2-{3-[(3-tert-butoxycarbonylamino-propyl)-methyl-amino]-propylamino}-3,4-dioxo-cyclobut-1-enylamino)-propyl]-methyl-amino}-propyl)-carbamic acid tert-butyl ester

3,3'-Diamino-N-methyldipropylamine

2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile