DL-2-N-tert-butoxycarbonylamino-2-(3-hydroxyphenyl)acetic acid

Base Information

Chemical Name:DL-2-N-tert-butoxycarbonylamino-2-(3-hydroxyphenyl)acetic acid
CAS No.:33130-90-4
Molecular Formula:C₁₃H₁₇NO₅
Molecular Weight:267.282
Hs Code.:

Synonyms:

Suppliers and Price of DL-2-N-tert-butoxycarbonylamino-2-(3-hydroxyphenyl)acetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Activate Scientific
(R)-alpha-(Boc-amino)-3-hydroxybenzeneacetic acid 95+% ee
5 g
$ 1040.00

Activate Scientific
(R)-alpha-(Boc-amino)-3-hydroxybenzeneacetic acid 95+% ee
1 g
$ 316.00

Acrotein
(R)-a-(Boc-amino)-3-hydroxybenzeneaceticacid 97%
0.5g
$ 220.00

ACHEMBLOCK
(R)-a-(Boc-amino)-3-hydroxybenzeneaceticacid 95%
5G
$ 880.00

ACHEMBLOCK
(R)-a-(Boc-amino)-3-hydroxybenzeneaceticacid 95%
1G
$ 325.00

Total 7 raw suppliers

Chemical Property of DL-2-N-tert-butoxycarbonylamino-2-(3-hydroxyphenyl)acetic acid

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

(R)-alpha-(Boc-amino)-3-hydroxybenzeneacetic acid 95+% ee ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of DL-2-N-tert-butoxycarbonylamino-2-(3-hydroxyphenyl)acetic acid

There total 5 articles about DL-2-N-tert-butoxycarbonylamino-2-(3-hydroxyphenyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 41840-28-2
S-tert-butoxycarbonyl-4,6-dimethyl-2-mercaptopyrimidine

: 71301-82-1
(S)-3-hydroxyphenylglycine

: 46988-94-7,33130-90-4
(2S)-(+)-N-tert-Butoxycarbonyl-2-(3-hdroxyphenyl)glycin

Guidance literature:: With triethylamine; In 1,4-dioxane; water; for 23h; Ambient temperature;

Reference yield:

: active-carbon

: 24424-99-5
di-tert-butyl dicarbonate

: 31932-87-3
D-α-amino-m-hydroxyphenylacetic acid

: 33130-90-4
DL-2-N-tert-butoxycarbonylamino-2-(3-hydroxyphenyl)acetic acid

Guidance literature:: With triethylamine; In tetrahydrofuran;

Reference yield:

: 108647-55-8
(2S)-(+)-2-(3-Methoxyphenyl)glycin

: 46988-94-7,33130-90-4
(2S)-(+)-N-tert-Butoxycarbonyl-2-(3-hdroxyphenyl)glycin

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / 48percent HBr / 4 h / 130 - 140 °C

2: 87 percent / NEt₃ / H₂O; dioxane / 23 h / Ambient temperature

With hydrogen bromide; triethylamine; In 1,4-dioxane; water;