Zn(tta)2(tmeda)

Base Information

• Chemical Name: Zn(tta)2(tmeda)
• CAS No.: 873585-38-7
• Molecular Formula: C₂₂H₂₄F₆N₂O₄S₂Zn
• Molecular Weight: 623.956
• Mol file: 873585-38-7.mol

Synonyms:

Chemical Property of Zn(tta)2(tmeda)

Chemical Property:

• Melting Point: 128-130 °C

Purity/Quality:

99% ^*data from raw suppliers

Bis[4,4,4-trifluoro-1-(2-thienyl-1,3-butanedionato]zinc TMEDA adduct, 99% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Zn(tta)2(tmeda)

There total 1 articles about Zn(tta)2(tmeda) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

1,1,1-trifluoro-4-(2-thienyl)butane-2,4-dione (326-91-0) + N,N,N,N,-tetramethylethylenediamine (110-18-9) + zinc(II) acetate dihydrate (5970-45-6) → Zn(tta)2(tmeda) (873585-38-7)

Guidance literature:

In dichloromethane; water; byproducts: CH3COOH, H2O; addn. of aq. zinc salt to a soln. of ligands in CH2Cl2, stirring; addn. of EtOH, crystn., washing with pentane; elem. anal.;

DOI:10.1021/ic051175i

upstream raw materials:

1,1,1-trifluoro-4-(2-thienyl)butane-2,4-dione

N,N,N,N,-tetramethylethylenediamine

zinc(II) acetate dihydrate