Hexadecanoic acid (2R,3R,4R,5S,6R)-3,4-dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl ester

Base Information

Chemical Name:Hexadecanoic acid (2R,3R,4R,5S,6R)-3,4-dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl ester
CAS No.:86137-81-7
Molecular Formula:C₂₈H₅₂O₁₂
Molecular Weight:580.714
Hs Code.:

Hexadecanoic acid (2R,3R,4R,5S,6R)-3,4-dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl ester

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Chemical Property of Hexadecanoic acid (2R,3R,4R,5S,6R)-3,4-dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl ester

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Technology Process of Hexadecanoic acid (2R,3R,4R,5S,6R)-3,4-dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl ester

There total 2 articles about Hexadecanoic acid (2R,3R,4R,5S,6R)-3,4-dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 74058-64-3
1-(2-Thioxo-thiazolidin-3-yl)-hexadecan-1-one

: 86137-81-7
Hexadecanoic acid (2R,3R,4R,5S,6R)-3,4-dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl ester

Guidance literature:: With sodium hydride; In pyridine; for 3h; Ambient temperature;
DOI:10.1016/S0040-4039(00)81507-5

Reference yield:

: 112-67-4
n-hexadecanoyl chloride

: 86137-81-7
Hexadecanoic acid (2R,3R,4R,5S,6R)-3,4-dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / triethylamine / CH₂Cl₂ / 3 h / 0 - 5 °C

2: NaH / 1.) pyridine, 100-110 deg C, 1 h, 2.) room temp., 3 h

With sodium hydride; triethylamine; In dichloromethane;
DOI:10.1016/0040-4020(86)80009-6