2-(1,3-dioxolan-2-yl)-1-O-tolylethanone

Base Information

• Chemical Name: 2-(1,3-dioxolan-2-yl)-1-O-tolylethanone
• CAS No.: 857195-93-8
• Molecular Formula: C₁₂H₁₄O₃
• Molecular Weight: 206.241
• Mol file: 857195-93-8.mol

Synonyms:

Chemical Property of 2-(1,3-dioxolan-2-yl)-1-O-tolylethanone

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

2-(1,3-Dioxolan-2-yl)-1-(2-methylphenyl)-ethanone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(1,3-dioxolan-2-yl)-1-O-tolylethanone

There total 2 articles about 2-(1,3-dioxolan-2-yl)-1-O-tolylethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1,3-DIOXOLANE (646-06-0) + 1-methyl-2-vinyl-benzene (611-15-4) → 2-(1,3-dioxolan-2-yl)-1-O-tolylethanone (857195-93-8)

Guidance literature:

With diatomite-supported manganese oxide nanoparticles; air; at 80 ℃; for 12h; regioselective reaction;

DOI:10.1021/jo2026367

Reference yield:

→ 2-(1,3-dioxolan-2-yl)-1-O-tolylethanone (857195-93-8)

Guidance literature:

With potassium carbonate; ethylene glycol;

upstream raw materials:

1,3-DIOXOLANE

1-methyl-2-vinyl-benzene

Refernces

• 1、 Cheng, Kai,Huang, Lehao,Zhang, Yuhong. "CuBr-mediated oxyalkylation of vinylarenes under aerobic conditions via cleavage of sp3 C-H bonds α to oxygen". supporting information; experimental part. p. 2908 - 2911. Retrieved 2009/12/06.