1,3,5-trimethyl-2,4,6-tris(4-formylphenyl)benzene

Base Information

Chemical Name:1,3,5-trimethyl-2,4,6-tris(4-formylphenyl)benzene
CAS No.:2195343-70-3
Molecular Formula:C₃₀H₂₄O₃
Molecular Weight:432.519
Hs Code.:

Synonyms:

Suppliers and Price of 1,3,5-trimethyl-2,4,6-tris(4-formylphenyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
5'-(4-Formylphenyl)-2',4',6'-trimethyl-[1,1':3',1''-terphenyl]-4,4''-dicarbaldehyde 98%
1g
$ 218.00

Arctom
5'-(4-Formylphenyl)-2',4',6'-trimethyl-[1,1':3',1''-terphenyl]-4,4''-dicarbaldehyde 98%
250mg
$ 75.00

Arctom
5'-(4-Formylphenyl)-2',4',6'-trimethyl-[1,1':3',1''-terphenyl]-4,4''-dicarbaldehyde 98%
100mg
$ 45.00

Total 11 raw suppliers

Chemical Property of 1,3,5-trimethyl-2,4,6-tris(4-formylphenyl)benzene

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

5'-(4-Formylphenyl)-2',4',6'-trimethyl-[1,1':3',1''-terphenyl]-4,4''-dicarbaldehyde 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3,5-trimethyl-2,4,6-tris(4-formylphenyl)benzene

There total 3 articles about 1,3,5-trimethyl-2,4,6-tris(4-formylphenyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 19025-36-6
2,4,6-triiodomesitylene

: 87199-17-5
4-formylphenylboronic acid,

: 2195343-70-3
1,3,5-trimethyl-2,4,6-tris(4-formylphenyl)benzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; at 80 ℃; for 48h; Inert atmosphere;
DOI:10.1002/anie.201708246

Reference yield:

: 608-72-0
2,4,6-tribromomesitylene

: 87199-17-5
4-formylphenylboronic acid,

: 2195343-70-3
1,3,5-trimethyl-2,4,6-tris(4-formylphenyl)benzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; at 100 ℃; for 72h;
DOI:10.1021/jacs.0c03409 DOI:10.1021/jacs.1c12020

Reference yield:

: 108-67-8
1,3,5-trimethyl-benzene

: 2195343-70-3
1,3,5-trimethyl-2,4,6-tris(4-formylphenyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: bromine; iron(III) chloride / 2 h / Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane / 72 h / 100 °C

With iron(III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; potassium carbonate; In 1,4-dioxane;
DOI:10.1021/jacs.0c03409