dehydrobufotenine

Base Information

Chemical Name:dehydrobufotenine
CAS No.:17284-76-3
Molecular Formula:C₁₂H₁₅N₂O*I
Molecular Weight:330.168
Hs Code.:

Synonyms:

Suppliers and Price of dehydrobufotenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dehydrobufotenine

Chemical Property:

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Technology Process of dehydrobufotenine

There total 13 articles about dehydrobufotenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1236071-48-9
6-[(tert-butyldimethylsilyl)oxy]-1,3,4,5-tetrahydropyrrolo[4,3,2-de]quinoline

: 74-88-4
methyl iodide

: 17284-76-3
dehydrobufotenine

Guidance literature:: With sodium hydrogencarbonate; In methanol; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2010.04.081

Reference yield: 50.0%

: tert-butyl 6-methoxy-4,5-dihydropyrrolo[4,3,2-de]quinoline-1(3H)-carboxylate

: 74-88-4
methyl iodide

: 17284-76-3
dehydrobufotenine

Guidance literature:: tert-butyl 6-methoxy-4,5-dihydropyrrolo[4,3,2-de]quinoline-1(3H)-carboxylate; With boron tribromide; In dichloromethane; at -78 - 30 ℃; for 12h; Inert atmosphere;

With potassium hydrogencarbonate; In methanol; dichloromethane; at 0 ℃; for 1h;

methyl iodide; In methanol;

Reference yield:

: 173217-19-1
3-(2-Dimethylamino-ethyl)-4-iodo-5-methoxy-indole-1-carboxylic acid ethyl ester

: 17284-76-3
dehydrobufotenine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) ClCOOCHClMe, 2.) EtOH / 1.) dichloroethane, reflux, 12 h, 2.) dichloroethane, reflux, 12 h

2: 82 percent / Et₃N, K₂CO₃, Pd(PPh₃)4 / toluene / 15 h / 200 °C

3: BBr₃ / CH₂Cl₂ / Ambient temperature

4: 1.) KHCO₃ / 1.) CH₂Cl₂, MeOH, from 0 deg C to RT, 1.5 h, 2.) MeOH, RT

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ethanol; carbonochloridic acid 1-chloro-ethyl ester; boron tribromide; potassium carbonate; potassium hydrogencarbonate; triethylamine; In dichloromethane; toluene;
DOI:10.1021/ja953080t