4-Methyl-N-picryl-2-aminophenol

Base Information

• Chemical Name: 4-Methyl-N-picryl-2-aminophenol
• CAS No.: 74716-60-2
• Molecular Formula: C₁₃H₁₀N₄O₇
• Molecular Weight: 334.245
• Mol file: 74716-60-2.mol

Synonyms:

Chemical Property of 4-Methyl-N-picryl-2-aminophenol

Chemical Property:

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-(2-HYDROXY-5-METHYLPHENYL)PICRYLAMINE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-Methyl-N-picryl-2-aminophenol

There total 5 articles about 4-Methyl-N-picryl-2-aminophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-2-nitrophenol (119-33-5) → 4-Methyl-N-picryl-2-aminophenol (74716-60-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium dithionite; aq. NaOH solution

2: sodium acetate; ethanol

With sodium hydroxide; sodium dithionite; ethanol; sodium acetate;

DOI:10.1039/jr9340000727

Reference yield:

2,4,6-trinitrochlorobenzene (88-88-0) + 3-amino-4-hydroxytoluene (95-84-1) → 4-Methyl-N-picryl-2-aminophenol (74716-60-2)

Guidance literature:

With ethanol; sodium acetate;

DOI:10.1039/jr9340000727

Reference yield:

2,4,6-trinitrochlorobenzene (88-88-0) + 3-amino-4-hydroxytoluene (95-84-1) → 4-Methyl-N-picryl-2-aminophenol (74716-60-2) + 2-picryloxy-5-methyl-aniline (876494-60-9)

Guidance literature:

With ethanol; potassium ethoxide;

DOI:10.1039/jr9340000727

upstream raw materials:

pyridine

2-picryloxy-5-methyl-aniline

1-methyl-4-nitrosobenzene

2,4,6-trinitrochlorobenzene