N-[1-(2-Naphthalenyl)ethyl]formamide

Base Information

• Chemical Name: N-[1-(2-Naphthalenyl)ethyl]formamide
• CAS No.: 273384-77-3
• Molecular Formula: C₁₃H₁₃NO
• Molecular Weight: 199.252
• Hs Code.: 2924297099
• Mol file: 273384-77-3.mol

Synonyms:

Chemical Property of N-[1-(2-Naphthalenyl)ethyl]formamide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

N-[1-(2-Naphthalenyl)ethyl]formamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[1-(2-Naphthalenyl)ethyl]formamide

There total 6 articles about N-[1-(2-Naphthalenyl)ethyl]formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-(2-Naphthyl)ethylamine (1201-74-7,3082-62-0,3906-16-9,64234-21-5) + formamide (77287-34-4,77287-35-5,60100-09-6) → N-(1-Naphthalen-2-yl-ethyl)-formamide (273384-77-3)

Guidance literature:

With sodium methylate; at 20 ℃; for 6h;

DOI:10.1016/j.tetlet.2012.12.009

Reference yield: 60.0%

formamide (77287-34-4,77287-35-5,60100-09-6) + methyl 2-naphthyl ketone (93-08-3) → N-(1-Naphthalen-2-yl-ethyl)-formamide (273384-77-3)

Guidance literature:

With formic acid; Inert atmosphere; Heating;

Reference yield:

ammonium formate (16712-16-6,64165-14-6,65387-22-6,70179-79-2,540-69-2) + methyl 2-naphthyl ketone (93-08-3) → N-(1-Naphthalen-2-yl-ethyl)-formamide (273384-77-3) + 2-(2-naphthyl)ethanol (7228-47-9)

Guidance literature:

With 4-methoxy-N-(1-(naphthalen-2-yl)ethylidene)aniline; In ethyl acetate; at 80 ℃; for 4h; chemoselective reaction;

DOI:10.1002/chem.201303541

upstream raw materials:

formic acid

methyl 2-naphthyl ketone

formamide

1-(2-Naphthyl)ethylamine

Downstream raw materials:

C₁₃H₁₃NO