Technology Process of 9-(n-butyl)imidazo[1,2-a]benzimidazole
There total 5 articles about 9-(n-butyl)imidazo[1,2-a]benzimidazole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,10-Phenanthroline; oxygen; copper diacetate; sodium acetate;
In
m-xylene;
at 155 ℃;
for 55h;
under 760.051 Torr;
DOI:10.1021/ol202884z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate
2: 1,10-Phenanthroline; oxygen; copper diacetate; sodium acetate / m-xylene / 55 h / 155 °C / 760.05 Torr
With
sodium tetrahydroborate; 1,10-Phenanthroline; oxygen; copper diacetate; sodium acetate;
In
m-xylene;
DOI:10.1021/ol202884z
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: copper(l) iodide; potassium carbonate / N,N-dimethyl-formamide / 24 h / 110 °C / Inert atmosphere
2.1: palladium 10% on activated carbon; hydrogen / ethanol / 4 h / 20 °C / 2280.15 Torr
3.1: trifluoroacetic acid / 0.08 h / 35 - 40 °C
3.2: 0.08 h
4.1: sodium tetrahydroborate
5.1: 1,10-Phenanthroline; oxygen; copper diacetate; sodium acetate / m-xylene / 55 h / 155 °C / 760.05 Torr
With
sodium tetrahydroborate; copper(l) iodide; 1,10-Phenanthroline; palladium 10% on activated carbon; hydrogen; oxygen; copper diacetate; sodium acetate; potassium carbonate; trifluoroacetic acid;
In
ethanol; N,N-dimethyl-formamide; m-xylene;
DOI:10.1021/ol202884z
