(2-isobutylphenyl)boronic acid

Base Information

Chemical Name:(2-isobutylphenyl)boronic acid
CAS No.:1651220-48-2
Molecular Formula:C₁₀H₁₅BO₂
Molecular Weight:178.039
Hs Code.:

Synonyms:

Suppliers and Price of (2-isobutylphenyl)boronic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (2-isobutylphenyl)boronic acid

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of (2-isobutylphenyl)boronic acid

There total 3 articles about (2-isobutylphenyl)boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 80304-54-7
(1-bromo-2-methylpropyl)benzene

: 1651220-48-2
(2-isobutylphenyl)boronic acid

Guidance literature:: (1-bromo-2-methylpropyl)benzene; With n-butyllithium; In tetrahydrofuran; n-heptane; at -72 - -70 ℃; for 1h; Inert atmosphere;

In tetrahydrofuran; n-heptane; at -72 - 20 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; n-heptane; for 1h; Inert atmosphere; Cooling with ice;

Reference yield:

: 71182-59-7
2-isobutylaniline

: 1651220-48-2
(2-isobutylphenyl)boronic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen bromide / water / 0.25 h / 20 °C

1.2: 3.75 h / -55 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; n-heptane / 1 h / -72 - -70 °C / Inert atmosphere

2.2: 2 h / -72 - 20 °C / Inert atmosphere

2.3: 1 h / Inert atmosphere; Cooling with ice

With n-butyllithium; hydrogen bromide; In tetrahydrofuran; n-heptane; water;

Reference yield:

: 615-36-1
2-bromoaniline

: 1651220-48-2
(2-isobutylphenyl)boronic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / tetrahydrofuran / 1.58 h / 55 °C / Inert atmosphere

1.2: 1.75 h / 39 °C / Inert atmosphere

1.3: 0.5 h / 32 - 33 °C / Inert atmosphere

2.1: hydrogen bromide / water / 0.25 h / 20 °C

2.2: 3.75 h / -55 - 20 °C

3.1: n-butyllithium / tetrahydrofuran; n-heptane / 1 h / -72 - -70 °C / Inert atmosphere

3.2: 2 h / -72 - 20 °C / Inert atmosphere

3.3: 1 h / Inert atmosphere; Cooling with ice

With n-butyllithium; hydrogen bromide; magnesium; In tetrahydrofuran; n-heptane; water;