Benzoylessigsaeure-<2.4-dimethyl-anilid>

Base Information

• Chemical Name: Benzoylessigsaeure-<2.4-dimethyl-anilid>
• CAS No.: 40624-73-5
• Molecular Formula: C₁₇H₁₇NO₂
• Molecular Weight: 267.327

Synonyms:

Chemical Property of Benzoylessigsaeure-<2.4-dimethyl-anilid>

Chemical Property:

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Technology Process of Benzoylessigsaeure-<2.4-dimethyl-anilid>

There total 1 articles about Benzoylessigsaeure-<2.4-dimethyl-anilid> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 3-oxo-3-phenylpropionate (94-02-0) + 2,4-Xylidine (95-68-1) → Benzoylessigsaeure-<2.4-dimethyl-anilid> (40624-73-5)

Guidance literature:

In 5,5-dimethyl-1,3-cyclohexadiene; at 140 ℃; for 4h;

DOI:10.1002/jhet.2256

Reference yield: 83.0%

Benzoylessigsaeure-<2.4-dimethyl-anilid> (40624-73-5) + Glutaraldehyde (111-30-8,29257-65-6,79215-57-9) + malononitrile (109-77-3) → 8-amino-3-benzoyl-1-(2,4-dimethylphenyl)-2-oxo-2,3,3a,3a1,4,5,6,6a-octahydro-1H-benzo[de][1,8]naphthyridine-3a1,7-dicarbonitrile

Guidance literature:

In ethanol; at 100 ℃; for 0.333333h; Microwave irradiation; Sealed tube;

DOI:10.1039/c4gc01469c

Reference yield:

Benzoylessigsaeure-<2.4-dimethyl-anilid> (40624-73-5) → 2-Hydroxy-6,8-dimethyl-4-phenyl-chinolin (93315-30-1)

Guidance literature:

With phosphorus pentoxide; phosphoric acid; at 100 ℃; for 6h;

DOI:10.1002/jhet.2256

upstream raw materials:

ethyl 3-oxo-3-phenylpropionate

2,4-Xylidine

Downstream raw materials:

2-Hydroxy-6,8-dimethyl-4-phenyl-chinolin

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