N-benzoyl-L-alanyl-L-alanine anilide

Base Information

Chemical Name:N-benzoyl-L-alanyl-L-alanine anilide
CAS No.:66412-01-9
Molecular Formula:C₁₉H₂₁N₃O₃
Molecular Weight:339.394
Hs Code.:

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Chemical Property of N-benzoyl-L-alanyl-L-alanine anilide

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Technology Process of N-benzoyl-L-alanyl-L-alanine anilide

There total 7 articles about N-benzoyl-L-alanyl-L-alanine anilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62-53-3
aniline

: 66412-01-9
N-benzoyl-L-alanyl-L-alanine anilide

Guidance literature:: Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h / 0 °C

1.2: 0 - 20 °C

2.1: trifluoroacetic acid / dichloromethane / 0.25 h / 20 °C

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.17 h

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane;
DOI:10.1002/chem.201502690

Reference yield:

: 126727-23-9,126787-11-9,68739-47-9
<1-(N-tert-butyloxycarbonyl)amino-1-methyl>-N-phenylacetamide

: 66412-01-9
N-benzoyl-L-alanyl-L-alanine anilide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 0.25 h / 20 °C

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.17 h

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid; In dichloromethane;
DOI:10.1002/chem.201502690

Reference yield:

: 98-88-4
benzoyl chloride

: 66412-01-9
N-benzoyl-L-alanyl-L-alanine anilide

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; pyridine / dichloromethane / 1.5 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 0.25 h / 20 °C

3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.17 h

With pyridine; dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid; In dichloromethane;
DOI:10.1002/chem.201502690