2,4-Dinitrophenylhydrazine-d3

Base Information

• Chemical Name: 2,4-Dinitrophenylhydrazine-d3
• CAS No.: 259824-49-2
• Molecular Formula: C₆H₆N₄O₄
• Molecular Weight: 201.114
• Mol file: 259824-49-2.mol

Synonyms:

Chemical Property of 2,4-Dinitrophenylhydrazine-d3

Chemical Property:

• Melting Point: 199-204°C
• Storage Temp.: Refrigerator
• Solubility.: Chloroform (Slightly)

Purity/Quality:

95% ^*data from raw suppliers

2,4-Dinitrophenylhydrazine-d3 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 2,4-Dinitrophenylhydrazine-d3 is a novel isotope-Labelled dinitrophenylhydrazines (DNPHs) and methods for their use in detecting and/or quantifying carbonyl groups in proteins and other analytes.

Technology Process of 2,4-Dinitrophenylhydrazine-d3

There total 2 articles about 2,4-Dinitrophenylhydrazine-d3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

d3-2,4-dinitrochlorobenzene → 3,5,6-d3-2,4-dinitrophenylhydrazine (259824-49-2)

Guidance literature:

With acetic acid; hydrazine;

DOI:10.1021/ac501309s

Reference yield:

chlorobenzene-d(5) (3114-55-4,59164-11-3) → 3,5,6-d3-2,4-dinitrophenylhydrazine (259824-49-2)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium nitrate; sulfuric acid

2: hydrazine; acetic acid

With sulfuric acid; acetic acid; potassium nitrate; hydrazine;

DOI:10.1021/ac501309s

Reference yield:

Malondialdehyde (542-78-9) + 3,5,6-d3-2,4-dinitrophenylhydrazine (259824-49-2) → C9H3(2)H3N4O4

Guidance literature:

With formic acid; In acetonitrile; at 40 ℃; for 2h; Darkness;

DOI:10.1021/ac501309s

upstream raw materials:

chlorobenzene-d⁽⁵⁾

Downstream raw materials:

C₉H₅⁽²⁾H₃N₄O₄