3-chloro-2-methoxylbenzonitrile

Base Information

• Chemical Name: 3-chloro-2-methoxylbenzonitrile
• CAS No.: 725718-12-7
• Molecular Formula: C₈H₆ClNO
• Molecular Weight: 167.595
• Hs Code.: 2926907090

Synonyms:

Chemical Property of 3-chloro-2-methoxylbenzonitrile

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

3-Chloro-2-methoxybenzonitrile ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-chloro-2-methoxylbenzonitrile

There total 3 articles about 3-chloro-2-methoxylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

silver cyanide (330660-35-0) + 1-chloro-3-methoxy-benzene (2845-89-8) → 4-chloro-2-methoxylbenzonitrile (100960-68-7) + 3-chloro-2-methoxylbenzonitrile (725718-12-7) + 2-chloro-4-methoxylbenzonitrile (127666-99-3)

Guidance literature:

With 1,1,1,3',3',3'-hexafluoro-propanol; silver(I) acetate; palladium diacetate; 5-chloro-3-nitropyridin-2-ol; at 100 ℃; for 24h; Overall yield = 64%; Overall yield = 21.7 mg; Sealed tube;

DOI:10.1002/chem.201805772

Reference yield:

silver cyanide (330660-35-0) + 2-Chloroanisole (766-51-8) → 3-chloro-2-methoxylbenzonitrile (725718-12-7) + 3-Chloro-4-methoxybenzonitrile (102151-33-7)

Guidance literature:

With 1,1,1,3',3',3'-hexafluoro-propanol; silver(I) acetate; palladium diacetate; 5-chloro-3-nitropyridin-2-ol; at 100 ℃; for 24h; Overall yield = 50%; Overall yield = 16.8 mg; Sealed tube;

DOI:10.1002/chem.201805772

Reference yield:

→ 3-chloro-2-methoxylbenzonitrile (725718-12-7)

Guidance literature:

With hydrogenchloride; copper;

upstream raw materials:

silver cyanide

2-Chloroanisole

1-chloro-3-methoxy-benzene

Downstream raw materials:

1-(3-chloro-2-methoxy-phenyl)-propan-1-one

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