9-acridinylnitrene

Base Information

• Chemical Name: 9-acridinylnitrene
• CAS No.: 1227269-49-9
• Molecular Formula: C₁₃H₈N₂
• Molecular Weight: 192.22
• Mol file: 1227269-49-9.mol

Synonyms:

Chemical Property of 9-acridinylnitrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-acridinylnitrene

There total 3 articles about 9-acridinylnitrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-Chloroacridine (1207-69-8) → 9-acridinylnitrene (1227269-49-9,90-45-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide / water; acetone / 0.01 h / Darkness; Microwave irradiation

2: 400 °C / Flash vacuum thermolysis

With sodium azide; In water; acetone;

DOI:10.1002/poc.1657

Reference yield:

2-(phenylamino)benzoic acid (91-40-7) → 9-acridinylnitrene (1227269-49-9,90-45-9)

Guidance literature:

Multi-step reaction with 3 steps

1: trichlorophosphate / 0.03 h / 100 °C / Microwave irradiation

2: sodium azide / water; acetone / 0.01 h / Darkness; Microwave irradiation

3: 400 °C / Flash vacuum thermolysis

With sodium azide; trichlorophosphate; In water; acetone;

DOI:10.1002/poc.1657

Reference yield:

9-azidoacridine (21330-56-3) → 9-acridinylnitrene (1227269-49-9,90-45-9)

Guidance literature:

at 400 ℃; Flash vacuum thermolysis;

DOI:10.1002/poc.1657

upstream raw materials:

9-Chloroacridine

2-(phenylamino)benzoic acid

9-azidoacridine