C₃₀H₄₂F₁₀N₂O₁₈

Base Information

Chemical Name:C₃₀H₄₂F₁₀N₂O₁₈
CAS No.:1582775-63-0
Molecular Formula:C₃₀H₄₂F₁₀N₂O₁₈
Molecular Weight:908.65
Hs Code.:

C<sub>30</sub>H<sub>42</sub>F<sub>10</sub>N<sub>2</sub>O<sub>18</sub>

Synonyms:

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Chemical Property of C₃₀H₄₂F₁₀N₂O₁₈

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Technology Process of C₃₀H₄₂F₁₀N₂O₁₈

There total 21 articles about C₃₀H₄₂F₁₀N₂O₁₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 212137-54-7
uridine 5'-diphospho-2-deoxy-2-trifluoroacetamido-α-D-glucopyranoside

: 1582775-57-2
C₂₂H₃₂F₇NO₁₃

: 1582775-63-0
C₃₀H₄₂F₁₀N₂O₁₈

Guidance literature:: With Escherichia coli glycosyltransferase; manganese(ll) chloride; In aq. buffer; at 20 ℃; pH=7.2; Enzymatic reaction;
DOI:10.1021/ol500738g

Reference yield:

: 1078691-95-8
(+)-D-glucosamine hydrochloride

: 1582775-63-0
C₃₀H₄₂F₁₀N₂O₁₈

Guidance literature:: Multi-step reaction with 14 steps

1.1: sodium azide; trifluoromethylsulfonic anhydride; copper(II) sulfate; triethylamine / acetonitrile; water / 0 - 20 °C

2.1: Amberlite resin (H⁺) / 72 h / Reflux; Inert atmosphere

3.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

4.1: pyridine; dmap / 0 - 20 °C / Inert atmosphere

5.1: sodium methylate / methanol / 0 - 20 °C / Inert atmosphere

6.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

6.2: 20 °C / Inert atmosphere

7.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2 h / 0 °C / Inert atmosphere

8.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

8.2: 2 h / 0 - 20 °C / Inert atmosphere

9.1: pyridine; hydrogen fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

10.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane; water / 20 °C

11.1: dihydrogen peroxide; lithium hydroxide / water; tetrahydrofuran / -5 - 20 °C

11.2: 0 - 20 °C

12.1: palladium 10% on activated carbon; hydrogen / methanol / 72 h / 20 °C

13.1: triethylamine / water; tetrahydrofuran / 20 °C

14.1: Escherichia coli glycosyltransferase; manganese(ll) chloride / aq. buffer / 20 °C / pH 7.2 / Enzymatic reaction

With pyridine; triethylsilane; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium azide; trifluoromethylsulfonic anhydride; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; boron trifluoride diethyl etherate; Escherichia coli glycosyltransferase; hydrogen fluoride; hydrogen; dihydrogen peroxide; sodium methylate; sodium hydride; toluene-4-sulfonic acid; copper(II) sulfate; triethylamine; manganese(ll) chloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol500738g

Reference yield:

: 2-azido-2-deoxy-D-glucose

: 1582775-63-0
C₃₀H₄₂F₁₀N₂O₁₈

Guidance literature:: Multi-step reaction with 13 steps

1.1: Amberlite resin (H⁺) / 72 h / Reflux; Inert atmosphere

2.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3.1: pyridine; dmap / 0 - 20 °C / Inert atmosphere

4.1: sodium methylate / methanol / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

5.2: 20 °C / Inert atmosphere

6.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2 h / 0 °C / Inert atmosphere

7.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

7.2: 2 h / 0 - 20 °C / Inert atmosphere

8.1: pyridine; hydrogen fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

9.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane; water / 20 °C

10.1: dihydrogen peroxide; lithium hydroxide / water; tetrahydrofuran / -5 - 20 °C

10.2: 0 - 20 °C

11.1: palladium 10% on activated carbon; hydrogen / methanol / 72 h / 20 °C

12.1: triethylamine / water; tetrahydrofuran / 20 °C

13.1: Escherichia coli glycosyltransferase; manganese(ll) chloride / aq. buffer / 20 °C / pH 7.2 / Enzymatic reaction

With pyridine; triethylsilane; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; boron trifluoride diethyl etherate; Escherichia coli glycosyltransferase; hydrogen fluoride; hydrogen; dihydrogen peroxide; sodium methylate; sodium hydride; toluene-4-sulfonic acid; triethylamine; manganese(ll) chloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol500738g