C₂₅H₂₃F₃N₂O₄S

Base Information

Chemical Name:C₂₅H₂₃F₃N₂O₄S
CAS No.:1620818-61-2
Molecular Formula:C₂₅H₂₃F₃N₂O₄S
Molecular Weight:504.53
Hs Code.:

C<sub>25</sub>H<sub>23</sub>F<sub>3</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:

Suppliers and Price of C₂₅H₂₃F₃N₂O₄S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₅H₂₃F₃N₂O₄S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₅H₂₃F₃N₂O₄S

There total 4 articles about C₂₅H₂₃F₃N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36455-21-7
3-benzyloxy-4-methoxyphenylethylamine

: 1620818-61-2
C₂₅H₂₃F₃N₂O₄S

: C₂₅H₂₃F₃N₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium 10% on activated carbon; hydrogen / methanol / 18 h / 20 °C / Inert atmosphere

2.1: triethylamine; potassium carbonate / chloroform; methanol / 0.08 h / 0 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

3.1: (R)-3,3′-bis(2,4,6-triisopropylphenyl)-BINOL-phosphoric acid; 1,1’-bi-2-naphthol / toluene; acetic acid / 0.17 h / Inert atmosphere

3.2: 80 °C / Inert atmosphere

4.1: chiralcel OD-H / n-heptane; isopropyl alcohol / Inert atmosphere; Resolution of racemate

With 1,1’-bi-2-naphthol; palladium 10% on activated carbon; (R)-3,3′-bis(2,4,6-triisopropylphenyl)-BINOL-phosphoric acid; hydrogen; potassium carbonate; triethylamine; In methanol; n-heptane; chloroform; acetic acid; isopropyl alcohol; toluene; 3.1: |Pictet-Spengler Synthesis;
DOI:10.1021/jo501099h

Reference yield:

: 3213-30-7
5-(2-amino-ethyl)-2-methoxy-phenol

: 1620818-61-2
C₂₅H₂₃F₃N₂O₄S

: C₂₅H₂₃F₃N₂O₄S

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; potassium carbonate / chloroform; methanol / 0.08 h / 0 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere

2.1: (R)-3,3′-bis(2,4,6-triisopropylphenyl)-BINOL-phosphoric acid; 1,1’-bi-2-naphthol / toluene; acetic acid / 0.17 h / Inert atmosphere

2.2: 80 °C / Inert atmosphere

3.1: chiralcel OD-H / n-heptane; isopropyl alcohol / Inert atmosphere; Resolution of racemate

With 1,1’-bi-2-naphthol; (R)-3,3′-bis(2,4,6-triisopropylphenyl)-BINOL-phosphoric acid; potassium carbonate; triethylamine; In methanol; n-heptane; chloroform; acetic acid; isopropyl alcohol; toluene; 2.1: |Pictet-Spengler Synthesis;
DOI:10.1021/jo501099h

Reference yield:

: 1620818-54-3
N-(2-nitrophenylsulfenyl)-β-(3-hydroxy-4-methoxyphenyl)ethylamine

: 1620818-61-2
C₂₅H₂₃F₃N₂O₄S

: C₂₅H₂₃F₃N₂O₄S

Guidance literature:: Multi-step reaction with 2 steps

1.1: (R)-3,3′-bis(2,4,6-triisopropylphenyl)-BINOL-phosphoric acid; 1,1’-bi-2-naphthol / toluene; acetic acid / 0.17 h / Inert atmosphere

1.2: 80 °C / Inert atmosphere

2.1: chiralcel OD-H / n-heptane; isopropyl alcohol / Inert atmosphere; Resolution of racemate

With 1,1’-bi-2-naphthol; (R)-3,3′-bis(2,4,6-triisopropylphenyl)-BINOL-phosphoric acid; In n-heptane; acetic acid; isopropyl alcohol; toluene; 1.1: |Pictet-Spengler Synthesis;
DOI:10.1021/jo501099h