Benzoyl chloride, 4-azido-3,5-dibromo-

Base Information

Chemical Name:Benzoyl chloride, 4-azido-3,5-dibromo-
CAS No.:140635-72-9
Molecular Formula:C7H2Br2ClN3O
Molecular Weight:339.373
Hs Code.:

Synonyms:

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Chemical Property of Benzoyl chloride, 4-azido-3,5-dibromo-

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Technology Process of Benzoyl chloride, 4-azido-3,5-dibromo-

There total 4 articles about Benzoyl chloride, 4-azido-3,5-dibromo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3282-10-8
methyl 3,5-dibromo-4-aminobenzoate

: 140635-72-9
4-Azido-3,5-dibromo-benzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) methanesulfonic acid, NaNO₂, 2.) aq. sodium azide / 1.) H₂O, 5 deg C, 24 h, 2.) H₂O, 5 deg C

2: 89 percent / KOH / methanol / 1 h / Ambient temperature

3: thionyl chloride / 5 h / Heating

With potassium hydroxide; thionyl chloride; sodium azide; methanesulfonic acid; sodium nitrite; In methanol;

Reference yield:

: 140635-68-3
methyl 4-azido-3,5-dibromo-benzoate

: 140635-72-9
4-Azido-3,5-dibromo-benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / KOH / methanol / 1 h / Ambient temperature

2: thionyl chloride / 5 h / Heating

With potassium hydroxide; thionyl chloride; In methanol;

Reference yield:

: 619-45-4
4-methoxycarbonyl aniline

: 140635-72-9
4-Azido-3,5-dibromo-benzoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / Br₂, triethylamine / acetic acid / 0.5 h / Heating

2: 1.) methanesulfonic acid, NaNO₂, 2.) aq. sodium azide / 1.) H₂O, 5 deg C, 24 h, 2.) H₂O, 5 deg C

3: 89 percent / KOH / methanol / 1 h / Ambient temperature

4: thionyl chloride / 5 h / Heating

With potassium hydroxide; thionyl chloride; sodium azide; methanesulfonic acid; bromine; triethylamine; sodium nitrite; In methanol; acetic acid;