benzyl 6-O-(benzyl 4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosylonate)-2-deoxy-2-<(R)-3-dodecanoyloxytetradecanamido>-3-O-<(R)-3-dodecanoyloxytetradecanoyl>-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 6-O-(benzyl 4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosylonate)-2-deoxy-2-<(R)-3-dodecanoyloxytetradecanamido>-3-O-<(R)-3-dodecanoyloxytetradecanoyl>-β-D-glucopyranoside
CAS No.:106022-70-2
Molecular Formula:C₈₈H₁₄₁NO₂₂
Molecular Weight:1565.08
Hs Code.:

benzyl 6-O-(benzyl 4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosylonate)-2-deoxy-2-<(R)-3-dodecanoyloxytetradecanamido>-3-O-<(R)-3-dodecanoyloxytetradecanoyl>-β-D-glucopyranoside

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Chemical Property of benzyl 6-O-(benzyl 4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosylonate)-2-deoxy-2-<(R)-3-dodecanoyloxytetradecanamido>-3-O-<(R)-3-dodecanoyloxytetradecanoyl>-β-D-glucopyranoside

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Technology Process of benzyl 6-O-(benzyl 4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosylonate)-2-deoxy-2-<(R)-3-dodecanoyloxytetradecanamido>-3-O-<(R)-3-dodecanoyloxytetradecanoyl>-β-D-glucopyranoside

There total 3 articles about benzyl 6-O-(benzyl 4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosylonate)-2-deoxy-2-<(R)-3-dodecanoyloxytetradecanamido>-3-O-<(R)-3-dodecanoyloxytetradecanoyl>-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106022-68-8
(R)-3-Dodecanoyloxy-tetradecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-dodecanoyloxy-tetradecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl ester

: 106022-64-4
benzyl 4,5,7,8-tetra-O-acetyl-2-bromo-3-deoxy-α-D-manno-2-octulosonate

: 106022-70-2
C₈₈H₁₄₁NO₂₂

: 106022-70-2
benzyl 6-O-(benzyl 4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosylonate)-2-deoxy-2-<(R)-3-dodecanoyloxytetradecanamido>-3-O-<(R)-3-dodecanoyloxytetradecanoyl>-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; mercury dibromide; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1248/cpb.34.2302

Reference yield:

: 106022-68-8
(R)-3-Dodecanoyloxy-tetradecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-dodecanoyloxy-tetradecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl ester

: 106022-64-4
benzyl 4,5,7,8-tetra-O-acetyl-2-bromo-3-deoxy-α-D-manno-2-octulosonate

: 106022-70-2
C₈₈H₁₄₁NO₂₂

: 106022-70-2
benzyl 6-O-(benzyl 4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosylonate)-2-deoxy-2-<(R)-3-dodecanoyloxytetradecanamido>-3-O-<(R)-3-dodecanoyloxytetradecanoyl>-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; mercury dibromide; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1248/cpb.34.2302

Reference yield:

: 106022-68-8
(R)-3-Dodecanoyloxy-tetradecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-dodecanoyloxy-tetradecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl ester

: 106022-64-4
benzyl 4,5,7,8-tetra-O-acetyl-2-bromo-3-deoxy-α-D-manno-2-octulosonate

: 106022-70-2
benzyl 6-O-(benzyl 4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosylonate)-2-deoxy-2-<(R)-3-dodecanoyloxytetradecanamido>-3-O-<(R)-3-dodecanoyloxytetradecanoyl>-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; mercury dibromide; Yield given. Multistep reaction; 1.) dichloromethane, 2 h, r.t; 2.) dichloromethane, 20 h, r.t.;
DOI:10.1248/cpb.35.4537