methyl ethyl(1-oxo-1-phenylpropan-2-yl)carbamate

Base Information

• Chemical Name: methyl ethyl(1-oxo-1-phenylpropan-2-yl)carbamate
• CAS No.: 30908-26-0
• Molecular Formula: C₁₃H₁₇NO₃
• Molecular Weight: 235.283
• Mol file: 30908-26-0.mol

Synonyms:

Chemical Property of methyl ethyl(1-oxo-1-phenylpropan-2-yl)carbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl ethyl(1-oxo-1-phenylpropan-2-yl)carbamate

There total 5 articles about methyl ethyl(1-oxo-1-phenylpropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-phenyl-propan-1-one (93-55-0) → methyl ethyl(1-oxo-1-phenylpropan-2-yl)carbamate (30908-26-0)

Guidance literature:

Multi-step reaction with 3 steps

1: bromine / dichloromethane

2: dichloromethane / 12 h

3: triethylamine / dichloromethane

With bromine; triethylamine; In dichloromethane;

DOI:10.3390/ijms20071524

Reference yield:

ethylamino-2-phenyl-1-propanone-1- (18259-37-5) + methyl chloroformate (79-22-1) → methyl ethyl(1-oxo-1-phenylpropan-2-yl)carbamate (30908-26-0)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.3390/ijms20071524

Reference yield:

→ methyl ethyl(1-oxo-1-phenylpropan-2-yl)carbamate (30908-26-0)

Guidance literature:

2-(Aethylamino)-propiophenonhydrochlorid, Methylchloroformiat, Na2CO3;

upstream raw materials:

ethylamino-2-phenyl-1-propanone-1-

methyl chloroformate

2-bromo-1-phenyl-1-propanone

1-phenyl-propan-1-one

Refernces