methyl 1-phenyl-3-ketobutyl sulfone

Base Information

• Chemical Name: methyl 1-phenyl-3-ketobutyl sulfone
• CAS No.: 79855-27-9
• Molecular Formula: C₁₁H₁₄O₃S
• Molecular Weight: 226.296
• Mol file: 79855-27-9.mol

Synonyms:

Chemical Property of methyl 1-phenyl-3-ketobutyl sulfone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of methyl 1-phenyl-3-ketobutyl sulfone

There total 2 articles about methyl 1-phenyl-3-ketobutyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-benzalacetone (1896-62-4) → methyl 1-phenyl-3-ketobutyl sulfone (79855-27-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Na₂S₂O₄ / 70 °C

2: HMPA

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium dithionite;

DOI:10.1021/jo00339a057

Reference yield:

sodium 1-phenyl-3-ketobutylsulfinate (79855-26-8) + methyl iodide (74-88-4) → methyl 1-phenyl-3-ketobutyl sulfone (79855-27-9)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide;

DOI:10.1021/jo00339a057

upstream raw materials:

sodium 1-phenyl-3-ketobutylsulfinate

methyl iodide

(E)-benzalacetone