C₁₉H₁₅NO₃

Base Information

Chemical Name:C₁₉H₁₅NO₃
CAS No.:1615685-40-9
Molecular Formula:C₁₉H₁₅NO₃
Molecular Weight:305.333
Hs Code.:

C<sub>19</sub>H<sub>15</sub>NO<sub>3</sub>

Synonyms:

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Chemical Property of C₁₉H₁₅NO₃

Chemical Property:

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Technology Process of C₁₉H₁₅NO₃

There total 12 articles about C₁₉H₁₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16426-64-5
2-bromo-4-nitrobenzoic acid

: 5-(3-benzoylpyrrol-1-yl)-2-hydroxymethylbenzaldehyde

: 1615685-40-9
C₁₉H₁₅NO₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: thionyl chloride / 4 h / Reflux

2.1: triethylamine / 1 h / 0 - 20 °C

3.1: tin(II) chloride dihdyrate / ethyl acetate / 4 h / Reflux

4.1: ethyl acetate / 4 h / Reflux

5.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

6.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C

6.2: 6 h

7.1: n-butyllithium / tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

7.2: Inert atmosphere

8.1: sodium tetrahydroborate / methanol / 0.5 h / 20 °C

9.1: triethylamine / dichloromethane / 20 °C

10.1: tin(IV) chloride / dichloromethane / -40 °C

11.1: sodium hydroxide / methanol; water / 0.25 h / 20 °C

12.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

13.1: boron tribromide / dichloromethane / -78 - 0 °C

13.2: 20 °C

With sodium tetrahydroborate; lithium borohydride; n-butyllithium; thionyl chloride; tin(II) chloride dihdyrate; boron tribromide; tin(IV) chloride; sodium hydride; triethylamine; pyridinium chlorochromate; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; mineral oil; 10.1: |Friedel-Crafts Acylation;
DOI:10.1016/j.ejmech.2014.04.079

Reference yield:

: 1615685-36-3
2-(methoxymethyl)-5-(pyrrol-1-yl)benzyl acetate

: 5-(3-benzoylpyrrol-1-yl)-2-hydroxymethylbenzaldehyde

: 1615685-40-9
C₁₉H₁₅NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: tin(IV) chloride / dichloromethane / -40 °C

2.1: sodium hydroxide / methanol; water / 0.25 h / 20 °C

3.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

4.1: boron tribromide / dichloromethane / -78 - 0 °C

4.2: 20 °C

With boron tribromide; tin(IV) chloride; pyridinium chlorochromate; sodium hydroxide; In methanol; dichloromethane; water; 1.1: |Friedel-Crafts Acylation;
DOI:10.1016/j.ejmech.2014.04.079

Reference yield:

: 1615685-37-4
2-(methoxymethyl)-5-(3-benzoylpyrrol-1-yl)benzyl acetate

: 5-(3-benzoylpyrrol-1-yl)-2-hydroxymethylbenzaldehyde

: 1615685-40-9
C₁₉H₁₅NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / methanol; water / 0.25 h / 20 °C

2.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

3.1: boron tribromide / dichloromethane / -78 - 0 °C

3.2: 20 °C

With boron tribromide; pyridinium chlorochromate; sodium hydroxide; In methanol; dichloromethane; water;
DOI:10.1016/j.ejmech.2014.04.079