5-nitro-3-(4-nitro-phenyl)-quinolin-2-ol

Base Information

Chemical Name:5-nitro-3-(4-nitro-phenyl)-quinolin-2-ol
CAS No.:108849-97-4
Molecular Formula:C₁₅H₉N₃O₅
Molecular Weight:311.254
Hs Code.:

Synonyms:

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Chemical Property of 5-nitro-3-(4-nitro-phenyl)-quinolin-2-ol

Chemical Property:

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Technology Process of 5-nitro-3-(4-nitro-phenyl)-quinolin-2-ol

There total 9 articles about 5-nitro-3-(4-nitro-phenyl)-quinolin-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106591-51-9
5-nitro-3-(4-nitro-phenyl)-quinoline-1-oxide

: 108849-97-4
5-nitro-3-(4-nitro-phenyl)-quinolin-2-ol

Guidance literature:: With acetic anhydride;
DOI:10.1021/jo01096a031

Reference yield:

: 612-58-8
3-methylquinoline

: 108849-97-4
5-nitro-3-(4-nitro-phenyl)-quinolin-2-ol

Guidance literature:: Multi-step reaction with 11 steps

1: concentrated sulfuric acid; nitric acid

2: CrO₃; MnO₂; aqueous H₂SO₄

3: SOCl₂ / Behandeln des Reaktionsprodukts mit wss. NaN₃ in Aceton

5: aqueous HCl / Erwaermen des Reaktionsprodukts mit Acetanhydrid in Benzol

6: aqueous HCl

7: HCl; NaNO₂; Na₂CO₃

8: benzene; toluene-4-sulfonic acid

9: sulfuric acid; nitric acid

10: acetic acid; water; hydrogen peroxide

11: acetic acid anhydride

With chromium(VI) oxide; hydrogenchloride; manganese(IV) oxide; thionyl chloride; sulfuric acid; water; dihydrogen peroxide; nitric acid; acetic anhydride; sodium carbonate; toluene-4-sulfonic acid; acetic acid; sodium nitrite; benzene;
DOI:10.1021/jo01096a031

Reference yield:

: 98589-84-5
5-nitro-[3]quinolylamine

: 108849-97-4
5-nitro-3-(4-nitro-phenyl)-quinolin-2-ol

Guidance literature:: Multi-step reaction with 5 steps

1: HCl; NaNO₂; Na₂CO₃

2: benzene; toluene-4-sulfonic acid

3: sulfuric acid; nitric acid

4: acetic acid; water; hydrogen peroxide

5: acetic acid anhydride

With hydrogenchloride; sulfuric acid; water; dihydrogen peroxide; nitric acid; acetic anhydride; sodium carbonate; toluene-4-sulfonic acid; acetic acid; sodium nitrite; benzene;
DOI:10.1021/jo01096a031