2-chloro-5-nitro-3-(4-nitro-phenyl)-quinoline

Base Information

Chemical Name:2-chloro-5-nitro-3-(4-nitro-phenyl)-quinoline
CAS No.:100914-19-0
Molecular Formula:C₁₅H₈ClN₃O₄
Molecular Weight:329.699
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-chloro-5-nitro-3-(4-nitro-phenyl)-quinoline

Chemical Property:

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Technology Process of 2-chloro-5-nitro-3-(4-nitro-phenyl)-quinoline

There total 11 articles about 2-chloro-5-nitro-3-(4-nitro-phenyl)-quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108849-97-4
5-nitro-3-(4-nitro-phenyl)-quinolin-2-ol

: 100914-19-0
2-chloro-5-nitro-3-(4-nitro-phenyl)-quinoline

Guidance literature:: With trichlorophosphate;
DOI:10.1021/jo01096a031

Reference yield:

: 612-58-8
3-methylquinoline

: 100914-19-0
2-chloro-5-nitro-3-(4-nitro-phenyl)-quinoline

Guidance literature:: Multi-step reaction with 12 steps

1: concentrated sulfuric acid; nitric acid

2: CrO₃; MnO₂; aqueous H₂SO₄

3: SOCl₂ / Behandeln des Reaktionsprodukts mit wss. NaN₃ in Aceton

5: aqueous HCl / Erwaermen des Reaktionsprodukts mit Acetanhydrid in Benzol

6: aqueous HCl

7: HCl; NaNO₂; Na₂CO₃

8: benzene; toluene-4-sulfonic acid

9: sulfuric acid; nitric acid

10: acetic acid; water; hydrogen peroxide

11: acetic acid anhydride

12: phosphoryl chloride

With chromium(VI) oxide; hydrogenchloride; manganese(IV) oxide; thionyl chloride; sulfuric acid; water; dihydrogen peroxide; nitric acid; acetic anhydride; sodium carbonate; toluene-4-sulfonic acid; acetic acid; sodium nitrite; trichlorophosphate; benzene;
DOI:10.1021/jo01096a031

Reference yield:

: 98589-84-5
5-nitro-[3]quinolylamine

: 100914-19-0
2-chloro-5-nitro-3-(4-nitro-phenyl)-quinoline

Guidance literature:: Multi-step reaction with 6 steps

1: HCl; NaNO₂; Na₂CO₃

2: benzene; toluene-4-sulfonic acid

3: sulfuric acid; nitric acid

4: acetic acid; water; hydrogen peroxide

5: acetic acid anhydride

6: phosphoryl chloride

With hydrogenchloride; sulfuric acid; water; dihydrogen peroxide; nitric acid; acetic anhydride; sodium carbonate; toluene-4-sulfonic acid; acetic acid; sodium nitrite; trichlorophosphate; benzene;
DOI:10.1021/jo01096a031