C₂₆H₂₇NO₆S

Base Information

Chemical Name:C₂₆H₂₇NO₆S
CAS No.:1451144-35-6
Molecular Formula:C₂₆H₂₇NO₆S
Molecular Weight:481.569
Hs Code.:

C<sub>26</sub>H<sub>27</sub>NO<sub>6</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₂₇NO₆S

Chemical Property:

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Technology Process of C₂₆H₂₇NO₆S

There total 2 articles about C₂₆H₂₇NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1451144-16-3
allyl 4-oxo-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylate

: 1451144-35-6
C₂₆H₂₇NO₆S

: C₂₆H₂₇NO₆S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / water; dichloromethane / 3 h / 0 °C

2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.33 h / 0 °C

2.2: 2 h / 0 - 20 °C

3.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (4S)-2-[2-(diphenylphosphino)phenyl]-4-isopropyl-4,5-dihydro-1,3-oxazole / toluene / 4 h / 80 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetra(n-butyl)ammonium hydrogensulfate; sodium hydride; (4S)-2-[2-(diphenylphosphino)phenyl]-4-isopropyl-4,5-dihydro-1,3-oxazole; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; toluene; mineral oil;
DOI:10.1071/CH13287

Reference yield:

: 1451144-21-0
allyl 9-((4-methoxyphenyl)sulfonyl)-4-oxo-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylate

: 1451144-35-6
C₂₆H₂₇NO₆S

: C₂₆H₂₇NO₆S

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.33 h / 0 °C

1.2: 2 h / 0 - 20 °C

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (4S)-2-[2-(diphenylphosphino)phenyl]-4-isopropyl-4,5-dihydro-1,3-oxazole / toluene / 4 h / 80 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hydride; (4S)-2-[2-(diphenylphosphino)phenyl]-4-isopropyl-4,5-dihydro-1,3-oxazole; In tetrahydrofuran; toluene; mineral oil;
DOI:10.1071/CH13287