C₃₆H₄₅N₅O₅

Base Information

Chemical Name:C₃₆H₄₅N₅O₅
CAS No.:1429922-25-7
Molecular Formula:C₃₆H₄₅N₅O₅
Molecular Weight:627.784
Hs Code.:

C<sub>36</sub>H<sub>45</sub>N<sub>5</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₄₅N₅O₅

Chemical Property:

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Technology Process of C₃₆H₄₅N₅O₅

There total 6 articles about C₃₆H₄₅N₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1432630-11-9
ethyl 5-(7-(1-ethyl-1,2,3,4-tetrahydroquinolin-7-yloxy)-2,2,4-trimethylquinolin-1(2H)-yl)pentanoate

: 1429922-25-7
C₃₆H₄₅N₅O₅

: 1429922-26-8
C₃₆H₄₅N₅O₅

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium 10% on activated carbon / ethyl acetate

2: hydrogenchloride / water / 0 °C / Inert atmosphere

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; In water; ethyl acetate;
DOI:10.1002/anie.201205369

Reference yield:

: 58196-33-1
7-hydroxy-1,2,3,4-tetrahydroquinoline

: 1429922-25-7
C₃₆H₄₅N₅O₅

: 1429922-26-8
C₃₆H₄₅N₅O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / 2 h / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: copper(l) iodide; potassium phosphate; 2-Picolinic acid / dimethyl sulfoxide / 85 °C / Sealed tube

3.1: toluene-4-sulfonic acid / 48 h / 20 °C / Inert atmosphere

4.1: sodium iodide; sodium carbonate / acetonitrile / 48 h / Inert atmosphere; Reflux

5.1: hydrogen; palladium 10% on activated carbon / ethyl acetate

6.1: hydrogenchloride / water / 0 °C / Inert atmosphere

With 2-Picolinic acid; hydrogenchloride; sodium tetrahydroborate; potassium phosphate; copper(l) iodide; palladium 10% on activated carbon; hydrogen; sodium carbonate; toluene-4-sulfonic acid; sodium iodide; In water; dimethyl sulfoxide; ethyl acetate; acetonitrile;
DOI:10.1002/anie.201205369

Reference yield:

: 22246-18-0
7-hydroxy-3,4-dihydro-2-(1H)-quinolinone

: 1429922-25-7
C₃₆H₄₅N₅O₅

: 1429922-26-8
C₃₆H₄₅N₅O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Cooling with ice; Reflux

2.1: sodium tetrahydroborate / 2 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: copper(l) iodide; potassium phosphate; 2-Picolinic acid / dimethyl sulfoxide / 85 °C / Sealed tube

4.1: toluene-4-sulfonic acid / 48 h / 20 °C / Inert atmosphere

5.1: sodium iodide; sodium carbonate / acetonitrile / 48 h / Inert atmosphere; Reflux

6.1: hydrogen; palladium 10% on activated carbon / ethyl acetate

7.1: hydrogenchloride / water / 0 °C / Inert atmosphere

With 2-Picolinic acid; hydrogenchloride; sodium tetrahydroborate; potassium phosphate; copper(l) iodide; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; sodium carbonate; toluene-4-sulfonic acid; sodium iodide; In tetrahydrofuran; water; dimethyl sulfoxide; ethyl acetate; acetonitrile;
DOI:10.1002/anie.201205369