α-bromo-cis-cinnamaldehyde seqtrans-oxime

Base Information

• Chemical Name: α-bromo-cis-cinnamaldehyde seqtrans-oxime
• CAS No.: 24247-46-9
• Molecular Formula: C₉H₈BrNO
• Molecular Weight: 226.073
• Mol file: 24247-46-9.mol

Synonyms:

Chemical Property of α-bromo-cis-cinnamaldehyde seqtrans-oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-bromo-cis-cinnamaldehyde seqtrans-oxime

There total 2 articles about α-bromo-cis-cinnamaldehyde seqtrans-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-2-bromo-3-phenylprop-2-enal (99686-39-2) → α-bromo-cis-cinnamaldehyde seqtrans-oxime (24247-46-9)

Guidance literature:

With hydroxylamine; alkal. wss. Loesung;

Reference yield:

α-bromo-cinnamaldehyde-(O-acetyl oxime ) → α-bromo-cinnamaldehyde-oxime (24247-46-9)

Guidance literature:

at 20 ℃;

Reference yield:

α-bromo-cis-cinnamaldehyde seqtrans-oxime (24247-46-9) → (Z)-2-bromo-3-phenylacrylic acid (15813-24-8)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus (V)-chloride; diethyl ether

2: aqueous sulfuric acid; acetic acid

With diethyl ether; phosphorus pentachloride; sulfuric acid; acetic acid;

upstream raw materials:

(E)-2-bromo-3-phenylprop-2-enal

Downstream raw materials:

(Z)-1-bromo-1-cyano-2-phenylethene

(E)-1-bromo-1-cyano-2-phenylethene

(Z)-2-bromo-3-phenylacrylic acid

β-ethoxy-cinnamonitrile